利用原位 XAFS、SAXS、XRD 及其组合技术进行电池表征的最新进展:从单一尺度到多尺度结构检测

Weidong Cheng, Mengyuan Zhao, Yuecheng Lai, Xin Wang, Huanyan Liu, Peng Xiao, Guang Mo, Bin Liu, Yunpeng Liu
{"title":"利用原位 XAFS、SAXS、XRD 及其组合技术进行电池表征的最新进展:从单一尺度到多尺度结构检测","authors":"Weidong Cheng,&nbsp;Mengyuan Zhao,&nbsp;Yuecheng Lai,&nbsp;Xin Wang,&nbsp;Huanyan Liu,&nbsp;Peng Xiao,&nbsp;Guang Mo,&nbsp;Bin Liu,&nbsp;Yunpeng Liu","doi":"10.1002/EXP.20230056","DOIUrl":null,"url":null,"abstract":"<p>Revealing and clarifying the chemical reaction processes and mechanisms inside the batteries will bring a great help to the controllable preparation and performance modulation of batteries. Advanced characterization techniques based on synchrotron radiation (SR) have accelerated the development of various batteries over the past decade. In situ SR techniques have been widely used in the study of electrochemical reactions and mechanisms due to their excellent characteristics. Herein, the three most wide and important synchrotron radiation techniques used in battery research were systematically reviewed, namely X-ray absorption fine structure (XAFS) spectroscopy, small-angle X-ray scattering (SAXS), and X-ray diffraction (XRD). Special attention is paid to how these characterization techniques are used to understand the reaction mechanism of batteries and improve the practical characteristics of batteries. Moreover, the in situ combining techniques advance the acquisition of single scale structure information to the simultaneous characterization of multiscale structures, which will bring a new perspective to the research of batteries. Finally, the challenges and future opportunities of SR techniques for battery research are featured based on their current development.</p>","PeriodicalId":72997,"journal":{"name":"Exploration (Beijing, China)","volume":"4 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-11-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/EXP.20230056","citationCount":"0","resultStr":"{\"title\":\"Recent advances in battery characterization using in situ XAFS, SAXS, XRD, and their combining techniques: From single scale to multiscale structure detection\",\"authors\":\"Weidong Cheng,&nbsp;Mengyuan Zhao,&nbsp;Yuecheng Lai,&nbsp;Xin Wang,&nbsp;Huanyan Liu,&nbsp;Peng Xiao,&nbsp;Guang Mo,&nbsp;Bin Liu,&nbsp;Yunpeng Liu\",\"doi\":\"10.1002/EXP.20230056\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Revealing and clarifying the chemical reaction processes and mechanisms inside the batteries will bring a great help to the controllable preparation and performance modulation of batteries. Advanced characterization techniques based on synchrotron radiation (SR) have accelerated the development of various batteries over the past decade. In situ SR techniques have been widely used in the study of electrochemical reactions and mechanisms due to their excellent characteristics. Herein, the three most wide and important synchrotron radiation techniques used in battery research were systematically reviewed, namely X-ray absorption fine structure (XAFS) spectroscopy, small-angle X-ray scattering (SAXS), and X-ray diffraction (XRD). Special attention is paid to how these characterization techniques are used to understand the reaction mechanism of batteries and improve the practical characteristics of batteries. Moreover, the in situ combining techniques advance the acquisition of single scale structure information to the simultaneous characterization of multiscale structures, which will bring a new perspective to the research of batteries. Finally, the challenges and future opportunities of SR techniques for battery research are featured based on their current development.</p>\",\"PeriodicalId\":72997,\"journal\":{\"name\":\"Exploration (Beijing, China)\",\"volume\":\"4 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-11-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://onlinelibrary.wiley.com/doi/epdf/10.1002/EXP.20230056\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Exploration (Beijing, China)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://onlinelibrary.wiley.com/doi/10.1002/EXP.20230056\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Exploration (Beijing, China)","FirstCategoryId":"1085","ListUrlMain":"https://onlinelibrary.wiley.com/doi/10.1002/EXP.20230056","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

揭示和阐明电池内部的化学反应过程和机制将为电池的可控制备和性能调控带来巨大帮助。过去十年间,基于同步辐射(SR)的先进表征技术加速了各种电池的发展。原位同步辐射技术因其卓越的特性被广泛应用于电化学反应和机理的研究。本文系统回顾了电池研究中使用最广泛、最重要的三种同步辐射技术,即 X 射线吸收精细结构(XAFS)光谱、小角 X 射线散射(SAXS)和 X 射线衍射(XRD)。其中特别关注了如何利用这些表征技术来了解电池的反应机理和改善电池的实用特性。此外,原位组合技术将单尺度结构信息的获取推进到多尺度结构的同步表征,这将为电池研究带来新的视角。最后,根据目前的发展情况,介绍了 SR 技术在电池研究中面临的挑战和未来的机遇。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Recent advances in battery characterization using in situ XAFS, SAXS, XRD, and their combining techniques: From single scale to multiscale structure detection

Recent advances in battery characterization using in situ XAFS, SAXS, XRD, and their combining techniques: From single scale to multiscale structure detection

Revealing and clarifying the chemical reaction processes and mechanisms inside the batteries will bring a great help to the controllable preparation and performance modulation of batteries. Advanced characterization techniques based on synchrotron radiation (SR) have accelerated the development of various batteries over the past decade. In situ SR techniques have been widely used in the study of electrochemical reactions and mechanisms due to their excellent characteristics. Herein, the three most wide and important synchrotron radiation techniques used in battery research were systematically reviewed, namely X-ray absorption fine structure (XAFS) spectroscopy, small-angle X-ray scattering (SAXS), and X-ray diffraction (XRD). Special attention is paid to how these characterization techniques are used to understand the reaction mechanism of batteries and improve the practical characteristics of batteries. Moreover, the in situ combining techniques advance the acquisition of single scale structure information to the simultaneous characterization of multiscale structures, which will bring a new perspective to the research of batteries. Finally, the challenges and future opportunities of SR techniques for battery research are featured based on their current development.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
CiteScore
17.20
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信