基于丁二烯橡胶和膨胀珍珠岩的复合材料的结构表征

IF 3 Q2 MATERIALS SCIENCE, COMPOSITES

Journal of Composites Science Pub Date : 2023-11-24 DOI:10.3390/jcs7120487

Nada Edres, Irada Buniyat-Zadeh, S. Turp, Mustafa Soylak, Solmaz Aliyeva, Nurlana Binnetova, Naila Guliyeva, Sevinj C. Mammadyarova, Rasim Alosmanov

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引用次数: 0

摘要

文章介绍了一种利用众所周知的矿物膨胀珍珠岩（EP）和工业聚合物丁二烯橡胶（BR）获得新型复合材料的方法。为了设计复合材料，对 BR 和 EP（以及 BR 和改性 EP）进行了联合氧化氯磷酸化反应，并对这些反应产生的改性物进行了进一步水解。利用傅立叶变换红外光谱、紫外-可见光谱、X 射线粉末衍射以及扫描电子显微镜和能量色散 X 射线分析，对所得样品的结构和形态进行了详细表征。对 EP 和 BR 分别进行了类似的改性反应，并进行了数据分析。

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Structural Characterization of Composites Based on Butadiene Rubber and Expanded Perlite

The article presents a method for obtaining new composites using the well-known mineral expanded perlite (EP), and the industrial polymer butadiene rubber (BR). For the design of composites, a joint oxidative chlorophosphorylation reaction of BR and EP (as well as BR and modified EP) was carried out, and the modifications resulting from these reactions were further hydrolyzed. The structure and morphology of the obtained samples were characterized in detail using Fourier transform infrared spectroscopy, ultraviolet-visible spectroscopy, X-ray powder diffraction, as well as scanning electron microscopy, and energy-dispersive X-ray analysis. EP and BR were separately modified with a similar reaction and characterized for data interpretation.

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