抛光技术对氧化锆增强硅酸锂陶瓷强度的影响

IF 1.8 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE
Ernesto Byron Benalcazar-Jalkh, Verena Souza Cunha, Edmara Tatiely Pedroso Bergamo, Larissa Marcia Martins Alves, Raphaelle Santos de Monteiro-Sousa, Tiago Moreira Bastos Campos, Ricardo Tanaka, Giovana de Assis Marcolino, Felipe Machado de Souza, Estevam Augusto Bonfante
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引用次数: 0

摘要

本研究的目的是评估上釉或抛光这两种表面处理技术与原切割状态相比对氧化锆增强硅酸锂陶瓷(ZLS)双轴挠性强度(BFS)的影响。圆柱体由 CAD/CAM 块铣削而成,切片后获得圆盘状试样(ISO6872:2015)。抛光和上釉试样按照制造商的说明进行处理。每种条件下都获得了 33 个试样,并进行了微观结构和 BFS/分形表征。对 BFS 和粗糙度数据分别采用 Weibull 统计法和方差分析单因子及 Tukey 后验法进行分析。虽然切割后的试样表面较粗糙,但在显微镜下观察到抛光和上釉的 ZLS 表面较光滑,并通过表面粗糙度评估得到了证实。X 射线光谱显示,所有组的试样都具有玻璃相,而原样切割和抛光试样则具有偏硅酸、二硅酸锂和磷酸锂的特征峰。上釉试样比抛光试样和原切割试样显示出更高的特征强度,但两者并无显著差异。虽然抛光试样的 Weibull 模量高于切割试样,但在统计上,上釉试样和抛光试样之间以及上釉试样和切割试样之间并无明显差异。上釉后的 ZLS 具有更高的强度,与原切割状态相比,抛光提高了材料的结构可靠性。两种表面处理技术都同样降低了表面粗糙度。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Finishing technique effect on strength of zirconia-reinforced lithium silicate ceramic

The aim of this study was to evaluate the effect of two finishing techniques, glazing or polishing, in comparison with the as-cut condition, on the biaxial-flexural-strength (BFS) of a zirconia-reinforced lithium silicate ceramic (ZLS). Cylinders were milled from CAD/CAM blocks and sliced to obtain disc-shaped specimens (ISO6872:2015). Polished and glazed specimens were processed following the manufacturer's instructions. Thirty-three specimens were obtained for each condition and microstructural and BFS/fractographic characterizations were performed. BFS and roughness data were analyzed using Weibull statistics and ANOVA one-way with Tukey post-hoc test, respectively. While a rougher surface was observed for as-cut specimens, smoother surfaces were observed for polished and glazed ZLS at microscopical evaluation and confirmed through surface-roughness evaluation. X-ray spectra depicted a glass phase for all groups and characteristic metasilicate, lithium disilicate, and lithium phosphate peaks for the as-cut and polished specimens. Glazed specimens showed higher characteristic strength than polished and as-cut specimens, which did not differ significantly. While higher Weibull-modulus was observed for the polished than for the as-cut specimens, no statistically significant differences were noted between glazed and polished, and between glazed and as-cut specimens. ZLS presents higher strength when glazed, and polishing increases the structural reliability of the material relative to the as-cut condition. Both finishing techniques reduced surface roughness similarly.

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来源期刊
European Journal of Oral Sciences
European Journal of Oral Sciences 医学-牙科与口腔外科
CiteScore
3.50
自引率
5.30%
发文量
61
审稿时长
2 months
期刊介绍: The European Journal of Oral Sciences is an international journal which publishes original research papers within clinical dentistry, on all basic science aspects of structure, chemistry, developmental biology, physiology and pathology of relevant tissues, as well as on microbiology, biomaterials and the behavioural sciences as they relate to dentistry. In general, analytical studies are preferred to descriptive ones. Reviews, Short Communications and Letters to the Editor will also be considered for publication. The journal is published bimonthly.
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