{"title":"纺织和高分子复合材料用新型木纤维素纤维的提取与表征","authors":"Divya Sundarraj, Grace Annapoorani Soundarajan, Indran Suyambulingam, Divya Divakaran, Sanjay Mavinkere Rangappa, Suchart Siengchin","doi":"10.47836/pjst.31.s1.07","DOIUrl":null,"url":null,"abstract":"Natural fibers derived from cellulose and ligno-celluloses materials have many advantages, such as being renewable, low density, inexhaustible, and cheap rather than synthetic fibers. Researchers and scientists are searching for a new fiber source that can be processed environmentally sustainable. The aim is to produce an organic and Eco-friendly product. The present investigation aims to extract and characterize ligno-cellulosic fiber from the seedpod of Wrightia tinctoria (WT) and Cebia pentandra (CP) plants. The extraction of WT fibers (WTFs) and CP fibers (CPFs) was carried out using the hand-stripping method. The structural and functional Characterization of WTFs and CPFs were determined using Scanning Electron Microscope (SEM), Fourier Transform Infrared (FT-IR) spectroscopy, Chemical analysis, X-ray diffraction studies (XRD), and the thermal behavior of fibers determined by using Thermo Gravimetric Analysis (TGA). The results indicated that WTFs composed of 75% cellulose, 14% lignin, and 0.55% wax content were, as the CPFs were composed of 38% cellulose, 15% lignin, and wax content of 2.34%. The SEM micrograph confirms that both fibers were hollow structures with thin cell walls and luminous because of the wax content presence on the surface of the fiber. The crystallinity percentage of WTFs and CPFs was calculated from XRD studies and is valued at 62% and 52%. Thermo gravimetric analysis revealed that WTFs and CPFs were thermally stable up to 460°C and 350°C. The above characterization results confirm that WTFs and CPFs have a wide scope in textile and polymer composite applications.","PeriodicalId":46234,"journal":{"name":"Pertanika Journal of Science and Technology","volume":"135 2","pages":"0"},"PeriodicalIF":0.6000,"publicationDate":"2023-10-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Extraction and Characterization of Novel Ligno-Cellulosic Fiber from Wrightia tinctoria and Cebia pentandra Plant for Textile and Polymer Composite Applications\",\"authors\":\"Divya Sundarraj, Grace Annapoorani Soundarajan, Indran Suyambulingam, Divya Divakaran, Sanjay Mavinkere Rangappa, Suchart Siengchin\",\"doi\":\"10.47836/pjst.31.s1.07\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Natural fibers derived from cellulose and ligno-celluloses materials have many advantages, such as being renewable, low density, inexhaustible, and cheap rather than synthetic fibers. Researchers and scientists are searching for a new fiber source that can be processed environmentally sustainable. The aim is to produce an organic and Eco-friendly product. The present investigation aims to extract and characterize ligno-cellulosic fiber from the seedpod of Wrightia tinctoria (WT) and Cebia pentandra (CP) plants. The extraction of WT fibers (WTFs) and CP fibers (CPFs) was carried out using the hand-stripping method. The structural and functional Characterization of WTFs and CPFs were determined using Scanning Electron Microscope (SEM), Fourier Transform Infrared (FT-IR) spectroscopy, Chemical analysis, X-ray diffraction studies (XRD), and the thermal behavior of fibers determined by using Thermo Gravimetric Analysis (TGA). The results indicated that WTFs composed of 75% cellulose, 14% lignin, and 0.55% wax content were, as the CPFs were composed of 38% cellulose, 15% lignin, and wax content of 2.34%. The SEM micrograph confirms that both fibers were hollow structures with thin cell walls and luminous because of the wax content presence on the surface of the fiber. The crystallinity percentage of WTFs and CPFs was calculated from XRD studies and is valued at 62% and 52%. Thermo gravimetric analysis revealed that WTFs and CPFs were thermally stable up to 460°C and 350°C. 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引用次数: 0
摘要
与合成纤维相比,由纤维素和木质纤维素材料制成的天然纤维具有可再生、密度低、取之不尽、用之不竭、价格低廉等优点。研究人员和科学家们正在寻找一种新的纤维来源,可以对环境进行可持续的处理。其目的是生产一种有机和环保的产品。本研究的目的是提取和表征wright tia tinctoria (WT)和Cebia pentandra (CP)植物种子中的木质纤维素纤维。采用手剥法提取WT纤维(WTFs)和CP纤维(CPFs)。采用扫描电镜(SEM)、傅里叶变换红外光谱(FT-IR)、化学分析、x射线衍射(XRD)和热重分析(TGA)对wtf和CPFs的结构和功能进行了表征。结果表明:纤维素含量为75%、木质素含量为14%、蜡含量为0.55%的wfs,纤维素含量为38%、木质素含量为15%、蜡含量为2.34%的CPFs。扫描电镜证实,这两种纤维都是空心结构,细胞壁薄,由于纤维表面含有蜡而发光。wtf和CPFs的结晶度分别为62%和52%。热重分析表明,wtf和CPFs在460°C和350°C温度下均具有热稳定性。上述表征结果证实了wtf和CPFs在纺织和高分子复合材料中具有广泛的应用范围。
Extraction and Characterization of Novel Ligno-Cellulosic Fiber from Wrightia tinctoria and Cebia pentandra Plant for Textile and Polymer Composite Applications
Natural fibers derived from cellulose and ligno-celluloses materials have many advantages, such as being renewable, low density, inexhaustible, and cheap rather than synthetic fibers. Researchers and scientists are searching for a new fiber source that can be processed environmentally sustainable. The aim is to produce an organic and Eco-friendly product. The present investigation aims to extract and characterize ligno-cellulosic fiber from the seedpod of Wrightia tinctoria (WT) and Cebia pentandra (CP) plants. The extraction of WT fibers (WTFs) and CP fibers (CPFs) was carried out using the hand-stripping method. The structural and functional Characterization of WTFs and CPFs were determined using Scanning Electron Microscope (SEM), Fourier Transform Infrared (FT-IR) spectroscopy, Chemical analysis, X-ray diffraction studies (XRD), and the thermal behavior of fibers determined by using Thermo Gravimetric Analysis (TGA). The results indicated that WTFs composed of 75% cellulose, 14% lignin, and 0.55% wax content were, as the CPFs were composed of 38% cellulose, 15% lignin, and wax content of 2.34%. The SEM micrograph confirms that both fibers were hollow structures with thin cell walls and luminous because of the wax content presence on the surface of the fiber. The crystallinity percentage of WTFs and CPFs was calculated from XRD studies and is valued at 62% and 52%. Thermo gravimetric analysis revealed that WTFs and CPFs were thermally stable up to 460°C and 350°C. The above characterization results confirm that WTFs and CPFs have a wide scope in textile and polymer composite applications.
期刊介绍:
Pertanika Journal of Science and Technology aims to provide a forum for high quality research related to science and engineering research. Areas relevant to the scope of the journal include: bioinformatics, bioscience, biotechnology and bio-molecular sciences, chemistry, computer science, ecology, engineering, engineering design, environmental control and management, mathematics and statistics, medicine and health sciences, nanotechnology, physics, safety and emergency management, and related fields of study.