H. Koruk, H. O. Koc, S. B. Yurdaer, A. Besli, A. N. Pouliopoulos
{"title":"利用放置在试样界面处的球形物体的动态响应测量软质材料粘弹性的新方法","authors":"H. Koruk, H. O. Koc, S. B. Yurdaer, A. Besli, A. N. Pouliopoulos","doi":"10.1007/s11340-023-01004-2","DOIUrl":null,"url":null,"abstract":"Abstract Background There are several techniques to characterize the mechanical properties of soft materials, such as the indentation method and the method based on the application of a spherical object placed inside the sample. The indentation systems usually yield the elastic properties of materials and their mathematical models do not consider the inertia of the sample involved in motion and radiation damping, while placing an object inside the sample is not practical and this procedure can alter the mechanical properties of the sample for the method based on the application of a bubble/sphere placed inside the sample. Objective A new approach for the identification of the viscoelastic properties of soft materials using the dynamic response of a spherical object placed at the sample interface was proposed. Methods The spherical object placed at the sample interface was pressed using an electromagnet and the dynamic response of the spherical object was tracked using a high-speed camera, while the dynamic response of the spherical object placed at the sample interface was estimated using a comprehensive analytical model. The effects of the shear modulus, viscosity, Poisson’s ratio and density of the soft sample, the radius and density of the spherical object and the damping due to radiation were considered in this mathematical model. The shear modulus and viscosity of the soft sample were determined by matching the experimentally identified and theoretically estimated responses of the spherical object. Results The shear moduli and viscosities of the three phantoms with the gelatin mass ratios of 0.20, 0.25 and 0.29 were measured to be 3450, 4300 and 4950 Pa and 12.5, 14.0 and 15.0 Pa⋅s, respectively. The shear modulus and viscosity of the phantom increases as the gelatin mass ratio increases. The frequency of oscillations of the hemisphere placed at the phantom interface increases as the gelatin mass ratio increases due to stiffness increase. Conclusions After matching the experimental and theoretical steady-state displacements and amplitudes of oscillations of the hemisphere at the sample interface, the comparison of the experimentally identified and theoretically predicted frequency of oscillations further confirmed the identified material properties of the samples. The approach presented here is expected to provide valuable information on material properties in biomedical and industrial applications.","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":null,"pages":null},"PeriodicalIF":2.0000,"publicationDate":"2023-10-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"A New Approach for Measuring Viscoelastic Properties of Soft Materials Using the Dynamic Response of a Spherical Object Placed at the Sample Interface\",\"authors\":\"H. Koruk, H. O. Koc, S. B. Yurdaer, A. Besli, A. N. Pouliopoulos\",\"doi\":\"10.1007/s11340-023-01004-2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract Background There are several techniques to characterize the mechanical properties of soft materials, such as the indentation method and the method based on the application of a spherical object placed inside the sample. The indentation systems usually yield the elastic properties of materials and their mathematical models do not consider the inertia of the sample involved in motion and radiation damping, while placing an object inside the sample is not practical and this procedure can alter the mechanical properties of the sample for the method based on the application of a bubble/sphere placed inside the sample. Objective A new approach for the identification of the viscoelastic properties of soft materials using the dynamic response of a spherical object placed at the sample interface was proposed. Methods The spherical object placed at the sample interface was pressed using an electromagnet and the dynamic response of the spherical object was tracked using a high-speed camera, while the dynamic response of the spherical object placed at the sample interface was estimated using a comprehensive analytical model. The effects of the shear modulus, viscosity, Poisson’s ratio and density of the soft sample, the radius and density of the spherical object and the damping due to radiation were considered in this mathematical model. The shear modulus and viscosity of the soft sample were determined by matching the experimentally identified and theoretically estimated responses of the spherical object. Results The shear moduli and viscosities of the three phantoms with the gelatin mass ratios of 0.20, 0.25 and 0.29 were measured to be 3450, 4300 and 4950 Pa and 12.5, 14.0 and 15.0 Pa⋅s, respectively. The shear modulus and viscosity of the phantom increases as the gelatin mass ratio increases. The frequency of oscillations of the hemisphere placed at the phantom interface increases as the gelatin mass ratio increases due to stiffness increase. Conclusions After matching the experimental and theoretical steady-state displacements and amplitudes of oscillations of the hemisphere at the sample interface, the comparison of the experimentally identified and theoretically predicted frequency of oscillations further confirmed the identified material properties of the samples. The approach presented here is expected to provide valuable information on material properties in biomedical and industrial applications.\",\"PeriodicalId\":552,\"journal\":{\"name\":\"Experimental Mechanics\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":2.0000,\"publicationDate\":\"2023-10-13\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Experimental Mechanics\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1007/s11340-023-01004-2\",\"RegionNum\":3,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Experimental Mechanics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1007/s11340-023-01004-2","RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
A New Approach for Measuring Viscoelastic Properties of Soft Materials Using the Dynamic Response of a Spherical Object Placed at the Sample Interface
Abstract Background There are several techniques to characterize the mechanical properties of soft materials, such as the indentation method and the method based on the application of a spherical object placed inside the sample. The indentation systems usually yield the elastic properties of materials and their mathematical models do not consider the inertia of the sample involved in motion and radiation damping, while placing an object inside the sample is not practical and this procedure can alter the mechanical properties of the sample for the method based on the application of a bubble/sphere placed inside the sample. Objective A new approach for the identification of the viscoelastic properties of soft materials using the dynamic response of a spherical object placed at the sample interface was proposed. Methods The spherical object placed at the sample interface was pressed using an electromagnet and the dynamic response of the spherical object was tracked using a high-speed camera, while the dynamic response of the spherical object placed at the sample interface was estimated using a comprehensive analytical model. The effects of the shear modulus, viscosity, Poisson’s ratio and density of the soft sample, the radius and density of the spherical object and the damping due to radiation were considered in this mathematical model. The shear modulus and viscosity of the soft sample were determined by matching the experimentally identified and theoretically estimated responses of the spherical object. Results The shear moduli and viscosities of the three phantoms with the gelatin mass ratios of 0.20, 0.25 and 0.29 were measured to be 3450, 4300 and 4950 Pa and 12.5, 14.0 and 15.0 Pa⋅s, respectively. The shear modulus and viscosity of the phantom increases as the gelatin mass ratio increases. The frequency of oscillations of the hemisphere placed at the phantom interface increases as the gelatin mass ratio increases due to stiffness increase. Conclusions After matching the experimental and theoretical steady-state displacements and amplitudes of oscillations of the hemisphere at the sample interface, the comparison of the experimentally identified and theoretically predicted frequency of oscillations further confirmed the identified material properties of the samples. The approach presented here is expected to provide valuable information on material properties in biomedical and industrial applications.
期刊介绍:
Experimental Mechanics is the official journal of the Society for Experimental Mechanics that publishes papers in all areas of experimentation including its theoretical and computational analysis. The journal covers research in design and implementation of novel or improved experiments to characterize materials, structures and systems. Articles extending the frontiers of experimental mechanics at large and small scales are particularly welcome.
Coverage extends from research in solid and fluids mechanics to fields at the intersection of disciplines including physics, chemistry and biology. Development of new devices and technologies for metrology applications in a wide range of industrial sectors (e.g., manufacturing, high-performance materials, aerospace, information technology, medicine, energy and environmental technologies) is also covered.