{"title":"超快速退火铁基软磁纺丝带的TEM, HREM, L-TEM研究","authors":"","doi":"10.24425/amm.2023.145489","DOIUrl":null,"url":null,"abstract":"in the present work, we performed the ultra-rapid annealing (ura) process for amorphous Fe 78 ni 8 B 14 melt-spun ribbons in order to obtain fine excellent microstructure assuring the best soft magnetic properties. several microscopic methods mainly based on transmission electron microscopy (teM) and lorentz teM (l-teM) were applied for detailed studies of the microstructure and magnetic domains structure. the investigation revealed that the optimized parameters of the uRA process (500°C/0.5-5 s) lead to outstanding soft magnetic properties. A mixture containing close to 50% amorphous phase and 50% α-Fe nanocrystals of size up to 30 nm has been already obtained after annealing for 3 s. these annealing conditions appear to be the most suitable in terms of microstructure providing the best magnetic properties.","PeriodicalId":8304,"journal":{"name":"Archives of Metallurgy and Materials","volume":"31 11","pages":"0"},"PeriodicalIF":0.7000,"publicationDate":"2023-11-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"TEM, HREM, L-TEM Studies of Fe-Based Soft Magnetic Melt-Spun Ribbons Subjected to Ultra-Rapid Annealing Process\",\"authors\":\"\",\"doi\":\"10.24425/amm.2023.145489\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"in the present work, we performed the ultra-rapid annealing (ura) process for amorphous Fe 78 ni 8 B 14 melt-spun ribbons in order to obtain fine excellent microstructure assuring the best soft magnetic properties. several microscopic methods mainly based on transmission electron microscopy (teM) and lorentz teM (l-teM) were applied for detailed studies of the microstructure and magnetic domains structure. the investigation revealed that the optimized parameters of the uRA process (500°C/0.5-5 s) lead to outstanding soft magnetic properties. A mixture containing close to 50% amorphous phase and 50% α-Fe nanocrystals of size up to 30 nm has been already obtained after annealing for 3 s. these annealing conditions appear to be the most suitable in terms of microstructure providing the best magnetic properties.\",\"PeriodicalId\":8304,\"journal\":{\"name\":\"Archives of Metallurgy and Materials\",\"volume\":\"31 11\",\"pages\":\"0\"},\"PeriodicalIF\":0.7000,\"publicationDate\":\"2023-11-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Archives of Metallurgy and Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.24425/amm.2023.145489\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"METALLURGY & METALLURGICAL ENGINEERING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Archives of Metallurgy and Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.24425/amm.2023.145489","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
TEM, HREM, L-TEM Studies of Fe-Based Soft Magnetic Melt-Spun Ribbons Subjected to Ultra-Rapid Annealing Process
in the present work, we performed the ultra-rapid annealing (ura) process for amorphous Fe 78 ni 8 B 14 melt-spun ribbons in order to obtain fine excellent microstructure assuring the best soft magnetic properties. several microscopic methods mainly based on transmission electron microscopy (teM) and lorentz teM (l-teM) were applied for detailed studies of the microstructure and magnetic domains structure. the investigation revealed that the optimized parameters of the uRA process (500°C/0.5-5 s) lead to outstanding soft magnetic properties. A mixture containing close to 50% amorphous phase and 50% α-Fe nanocrystals of size up to 30 nm has been already obtained after annealing for 3 s. these annealing conditions appear to be the most suitable in terms of microstructure providing the best magnetic properties.
期刊介绍:
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