汽车用LTCC/粘合剂和alloy 42/粘合剂界面强度的表征和模拟

B. Ozturk, P. Lou, P. Gromala, C. Silber, K. Jansen, L. Ernst
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引用次数: 2

摘要

热固性粘合剂用作热和电接口。在汽车应用中,它们需要具有优异的附着力,因为分层可能会析出其他电、热或机械故障机制。大量的文献可用于研究成型化合物和各种材料界面。然而,很少有研究关注粘接界面的分层现象。原因很明显,在分层样品中不可能产生界面裂纹。在各种尝试中,胶粘剂出现了随机开裂。然而,在实际产品中也发现了界面裂缝,并真正形成了可靠性问题。但到目前为止,由于缺乏足够的界面强度数据,因此很难设计具有粘合界面的产品的可靠性。本文解决了上述问题。我们成功地获得了粘合剂与两种不同材料(例如低温涂层陶瓷(L TCC)和合金42)之间的界面分层。样品的制造过程与所研究的电子控制单元的制造过程相同。通过在制造过程中添加一个步骤,对要研究的界面进行分层启动的预处理,从而能够研究具有与实际产品相同加工条件的不同界面。所提出的试样制备方法和测试方法可用于确定电子控制单元中不同界面(包括脆性材料如L TCC)的临界粘附性能。在室温下,通过i型加载条件下的分层实验对试件进行了研究。得到的界面数据通过图像处理和j积分法的有限元建模进行解释。特别地,利用内聚区建模来验证不同界面的临界能量释放率。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Characterization and simulation of LTCC/adhesive and alloy 42/adhesive interface strength for automotive applications
Thermoset-based adhesives are used as thermal and electrical interfaces. In automotive applications, they are required to have excellent adhesion since delamination may precipitate other electrical, thermal or mechanical failure mechanisms. A vast amount of literature is available on the investigation of molding compounds and various material interfaces. However, only very few studies focus on delamination of adhesive interfaces. The reason is that apparently it was not possible to initiate an interface crack in a delamination sample. In various attempts, random cracking in the adhesive was obtained instead. Yet interface cracks are found in real products and really form a reliability issue. But so far the absence of adequate interface strength data makes it hardly possible to design for reliability of products with adhesive interfaces. The present paper solves the above problem. We succeeded to get an interface delamination between the adhesive and two different materials (e.g. Low temperature cofrred ceramic (L TCC) and alloy 42). The specimens are made by identical fabrications processes as during the fabrication of the electronic control unit under study. The interface to be investigated is preconditioned for delamination initiation, by adding a single step to the fabrication process, thus enabling the investigation of different interfaces that have the same processing conditions as the real product. The presented specimen preparation method and the testing methodology can be used for determination of critical adhesion properties of different interfaces (including brittle materials like L TCC) in electronic control units. Specimens are investigated by delamination experiments near Mode-I loading conditions at room temperature. The obtained interface data is interpreted via image processing and finite element modeling of the J-integral method. In particular, cohesive zone modeling is used to validate the critical energy release rates for different interfaces.
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