高压扭转前后钨铜复合材料的纳米压痕

T. Schöberl, I. Sabirov, R. Pippan
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引用次数: 5

摘要

摘要:对W-Cu复合材料在室温、200和400℃的剧烈塑性变形前后进行了纳米压痕实验。采用高压扭转(HPT)诱导应变。对于最高程度的变形,颗粒尺寸达到10 - 20纳米。铜的纳米硬度随变形量的增加而显著提高,而钨的纳米硬度仅略有提高。高温高温热处理时温度为400℃,铜的硬度明显降低,可能是高温高温热处理过程中发生了再结晶,但钨的硬度未受影响。随着粒径的减小,相邻材料对测量性能的影响增大,硬度和模量的分布也趋于分散。继续到更小的颗粒和晶粒尺寸,颗粒变得比缩进的尺寸小。因此,硬度和模量值反映了纯钨和纯铜的平均值。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Nanoindentation applied on a tungsten - copper composite before and after high-pressure torsion
Abstract Nanoindentation experiments were performed before and after severe plastic deformation of W–Cu composites at room temperature, 200, and 400 °C. The strains were induced by high-pressure torsion (HPT). For the highest degrees of deformation, a particle size of 10 – 20 nanometer was achieved. The nanohardness of copper increased remarkably with increasing deformation, the hardness of tungsten was enhanced only slightly. A temperature of 400 °C during HPT significantly lowered the Cu hardness, probably recrystallisation during HPT had taken place, the hardness of tungsten, however, kept unaffected. With decreasing particle size, the influence of the adjacent material on the measured properties increased as well as the scatter of hardness and modulus. Proceeding to verq small particle and grain sizes, the particles became smaller than the size of the indent. Thus, hardness and modulus values reflected some average over that of pure tungstef and copper.
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