纳米银的合成与表征

I. Prosycevas, Algimantas Juraitis, J. Puišo, G. Niaura, A. Guobienė, S. Tamulevičius, G. Balčaitis, A. Šileikaitė
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引用次数: 31

摘要

银纳米粒子以其独特的物理和化学性质受到了广泛的关注。单个银纳米粒子的表面等离子体共振和大的有效散射截面使它们成为分子标记的理想候选者,其中表面增强拉曼散射(SERS)等现象可以被利用。此外,银纳米颗粒最近被证明是一种很有前途的抗菌材料。本研究采用柠檬酸钠还原法制备银胶体。胶体银通过浸渍涂覆在聚合物基体上。x射线荧光光谱(XRF)、原子力显微镜(AFM)、紫外可见光谱(UV-VIS)和SERS表明,制备的结构包含金属晶体纳米银。银粒子吸收光谱中的表面等离子体共振峰在420 ~ 500 nm处出现吸收最大值。制备了具有选择性光性能的银-聚合物纳米复合材料结构。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and characterization of silver nanoparticles
Silver nanoparticles have received considerable attention due to their attractive physical and chemical properties. The surface plasmon resonance and large effective scattering cross section of individual silver nanoparticles make them ideal candidates for molecular labeling, where phenomena such as surface enhance Raman scattering (SERS) can be exploited. In addition, silver nanoparticles have recently been shown to be a promising antimicrobial material. In the present research silver colloid was produced by sodium citrate reduction. The colloidal silver was incorporated by dip-coating to the polymer substrate. X-Ray Fluorescence Spectroscopy (XRF), Atomic force microscopy (AFM), ultraviolet-visible spectroscopy (UV-VIS ) and SERS indicate that the produced structures include metallic crystalline silver nanoparticles. The surface plasmon resonance peak in absorption spectra of silver particles showed an absorption maximum at 420-500 nm. The silver - polymer nanocomposites structures with selective light properties as a result of plasmon resonance shifting in the UV-VIS wavelength region were produced.
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