共沉淀法合成ZnO和Zn0.5Mg0.5O纳米颗粒的抑菌研究

Swathi T, Nithya V D
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引用次数: 0

摘要

本研究采用简单、经济的共沉淀法合成了氧化锌(ZnO)和镁掺杂氧化锌(Zn0.5Mg0.5O)纳米颗粒。采用x射线衍射(XRD)、傅里叶变换红外光谱(FTIR)、场发射扫描电镜(FESEM)和能量色散x射线能谱(EDAX)对合成材料进行了表征。最后,分析了镁的掺杂对ZnO纳米粒子结构、形态和抗菌性能的影响。XRD结果表明,ZnO和Zn0.5Mg0.5O的平均晶粒尺寸分别为71 nm和36 nm,形成了六边形结构的ZnO。FTIR分析证实ZnO和Zn0.5Mg0.5O中存在可能的官能团。从FESEM图像可以看出,氧化锌中掺杂Mg后形成了球状颗粒,并出现了颗粒团聚现象。制备的纳米粒子的EDAX光谱显示了ZnO中的Zn, O和Zn0.5Mg0.5O中的Zn, Mg, O的组成。在ZnO和Zn0.5Mg0.5O的EDAX光谱中没有发现其他元素可以证实纯物质的形成。结果表明,ZnO和Zn0.5Mg0.5O对大肠杆菌有较好的抑制作用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Antibacterial study of ZnO and Zn0.5Mg0.5O nanoparticles synthesized by co-precipitation method
In the present study, zinc oxide (ZnO) and magnesium doped zinc oxide (Zn0.5Mg0.5O) nanoparticles were synthesized by simple and cost-effective co-precipitation method. The synthesized materials were characterized by X-ray Diffraction (XRD), Fourier Transform Infrared (FTIR) spectroscopy, Field Emission Scanning Electron Microscopy (FESEM) with Energy dispersive X-ray spectrum (EDAX). Finally, the effect of magnesium (Mg) doping on the structural, morphological and anti-bacterial property of ZnO nanoparticles was analyzed. From the XRD results, it was found that there was a formation of hexagonal structured ZnO and the average crystallite size of ZnO and Zn0.5Mg0.5O was calculated to be 71 nm and 36 nm respectively. The FTIR analysis confirmed the existence of possible functional groups in ZnO and Zn0.5Mg0.5O. There was formation of almost spherical shaped particles as evident from FESEM images and agglomeration of particles was observed upon doping Mg into ZnO. The EDAX spectra of the prepared nanoparticles provided the composition of Zn, O in ZnO and Zn, Mg, O in Zn0.5Mg0.5O. No other elements have been found in the EDAX spectra of ZnO and Zn0.5Mg0.5O that confirmed the formation of pure materials. Finally the anti-bacterial study demonstrated that ZnO and Zn0.5Mg0.5O was effective in inhibiting E. coli bacteria.
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