从稻壳中提取吸附剂材料的制备与表征

A. Rodríguez, Ana María Campos Rosario, Alejandro Pérez Flores
{"title":"从稻壳中提取吸附剂材料的制备与表征","authors":"A. Rodríguez, Ana María Campos Rosario, Alejandro Pérez Flores","doi":"10.21789/22561498.1515","DOIUrl":null,"url":null,"abstract":"Agricultural waste management for the production of materials with specific uses is important for the remediation of certain environmental problems. Rice husk, an abundantly agricultural waste in Colombia, could be a low cost adsorbent for molecules such as dyes or heavy metals in effluent streams. In this research, we address the production and characterization of rice husk ash obtained by chemical activation with phosphoric acid as an adsorbent material. The physical-chemical properties of the materials were evaluated using different characterization techniques, such as close analysis, iodine number, adsorption of methylene blue, adsorption-desorption of nitrogen, analysis of the functional groups on the surface of the adsorbent through infrared spectroscopy (ftir), as well as an analysis of the morphology with scanning electron microscopy (sem). The materials have a surface area around 320 m2 /g, which decreases depending on the amount of acid used in the activation. The pore size in the studied samples ranged between 4 and 12 nm, which suggest that mesoporous solids were obtained. Regarding the adsorption of methylene blue, results show that the production of the activated ashes from rice husk as adsorbent materials is viable, presenting a new opportunity for the use of materials considered as agricultural waste.","PeriodicalId":193519,"journal":{"name":"Revista Mutis","volume":"31 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2019-06-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Obtención y caracterización de materiales adsorbentes a partir de cascarilla de arroz\",\"authors\":\"A. Rodríguez, Ana María Campos Rosario, Alejandro Pérez Flores\",\"doi\":\"10.21789/22561498.1515\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Agricultural waste management for the production of materials with specific uses is important for the remediation of certain environmental problems. Rice husk, an abundantly agricultural waste in Colombia, could be a low cost adsorbent for molecules such as dyes or heavy metals in effluent streams. In this research, we address the production and characterization of rice husk ash obtained by chemical activation with phosphoric acid as an adsorbent material. The physical-chemical properties of the materials were evaluated using different characterization techniques, such as close analysis, iodine number, adsorption of methylene blue, adsorption-desorption of nitrogen, analysis of the functional groups on the surface of the adsorbent through infrared spectroscopy (ftir), as well as an analysis of the morphology with scanning electron microscopy (sem). The materials have a surface area around 320 m2 /g, which decreases depending on the amount of acid used in the activation. The pore size in the studied samples ranged between 4 and 12 nm, which suggest that mesoporous solids were obtained. Regarding the adsorption of methylene blue, results show that the production of the activated ashes from rice husk as adsorbent materials is viable, presenting a new opportunity for the use of materials considered as agricultural waste.\",\"PeriodicalId\":193519,\"journal\":{\"name\":\"Revista Mutis\",\"volume\":\"31 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-06-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Revista Mutis\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.21789/22561498.1515\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Revista Mutis","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21789/22561498.1515","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

农业废物管理用于生产具有特定用途的材料,对于补救某些环境问题很重要。稻壳是哥伦比亚的一种丰富的农业废弃物,它可以作为废水中染料或重金属等分子的低成本吸附剂。在本研究中,我们研究了以磷酸为吸附剂的化学活化稻壳灰的生产和表征。采用不同的表征技术,如密切分析、碘值、亚甲基蓝吸附、氮的吸附-解吸、红外光谱(ftir)分析吸附剂表面官能团以及扫描电子显微镜(sem)分析吸附剂的形貌,对材料的物理化学性质进行了评价。该材料的表面积约为320 m2 /g,根据活化中使用的酸的量而减小。研究样品的孔径在4 ~ 12 nm之间,表明得到了介孔固体。在吸附亚甲基蓝方面,研究结果表明,稻壳活化灰作为吸附材料是可行的,为农业废弃物的利用提供了新的机遇。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Obtención y caracterización de materiales adsorbentes a partir de cascarilla de arroz
Agricultural waste management for the production of materials with specific uses is important for the remediation of certain environmental problems. Rice husk, an abundantly agricultural waste in Colombia, could be a low cost adsorbent for molecules such as dyes or heavy metals in effluent streams. In this research, we address the production and characterization of rice husk ash obtained by chemical activation with phosphoric acid as an adsorbent material. The physical-chemical properties of the materials were evaluated using different characterization techniques, such as close analysis, iodine number, adsorption of methylene blue, adsorption-desorption of nitrogen, analysis of the functional groups on the surface of the adsorbent through infrared spectroscopy (ftir), as well as an analysis of the morphology with scanning electron microscopy (sem). The materials have a surface area around 320 m2 /g, which decreases depending on the amount of acid used in the activation. The pore size in the studied samples ranged between 4 and 12 nm, which suggest that mesoporous solids were obtained. Regarding the adsorption of methylene blue, results show that the production of the activated ashes from rice husk as adsorbent materials is viable, presenting a new opportunity for the use of materials considered as agricultural waste.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信