{"title":"HPLC/MS法分析阿特诺酸芝麻油溶液的一步萃取法、样品制备方法[乙腈萃取阿特诺酸芝麻油，HPLC/MS法]","authors":"Stanislav V. Yefimov, P.B.F. Gil","doi":"10.36346/sarjps.2022.v04i01.003","DOIUrl":null,"url":null,"abstract":"The extraction of altrenogest with acetonitrile from sesame oil is not an easy task due to the formation of a stable emulsion. The problem of extracting more than 99% of altrenogest from sesame oil with acetonitrile was solved. The optimal ratio of extractant to extractor was established. This approach allowed for a quantitative analysis of altrenogest in sesame oil solutions by HPLC/MS. A generalization of the proposed approach to cases of altrenogest extraction from stable emulsions was discussed.","PeriodicalId":244449,"journal":{"name":"South Asian Research Journal of Pharmaceutical Sciences","volume":"53 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2022-02-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"One Step Extraction Method, Sample Preparation Procedure for HPLC/MS Analysis of Altrenogest Sesame Oil Solutions [Extraction of altrenogest from sesame oil with acetonitrile, HPLC/MS]\",\"authors\":\"Stanislav V. Yefimov, P.B.F. Gil\",\"doi\":\"10.36346/sarjps.2022.v04i01.003\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The extraction of altrenogest with acetonitrile from sesame oil is not an easy task due to the formation of a stable emulsion. The problem of extracting more than 99% of altrenogest from sesame oil with acetonitrile was solved. The optimal ratio of extractant to extractor was established. This approach allowed for a quantitative analysis of altrenogest in sesame oil solutions by HPLC/MS. A generalization of the proposed approach to cases of altrenogest extraction from stable emulsions was discussed.\",\"PeriodicalId\":244449,\"journal\":{\"name\":\"South Asian Research Journal of Pharmaceutical Sciences\",\"volume\":\"53 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-02-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"South Asian Research Journal of Pharmaceutical Sciences\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.36346/sarjps.2022.v04i01.003\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"South Asian Research Journal of Pharmaceutical Sciences","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.36346/sarjps.2022.v04i01.003","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
One Step Extraction Method, Sample Preparation Procedure for HPLC/MS Analysis of Altrenogest Sesame Oil Solutions [Extraction of altrenogest from sesame oil with acetonitrile, HPLC/MS]
The extraction of altrenogest with acetonitrile from sesame oil is not an easy task due to the formation of a stable emulsion. The problem of extracting more than 99% of altrenogest from sesame oil with acetonitrile was solved. The optimal ratio of extractant to extractor was established. This approach allowed for a quantitative analysis of altrenogest in sesame oil solutions by HPLC/MS. A generalization of the proposed approach to cases of altrenogest extraction from stable emulsions was discussed.
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