{"title":"As2S5与CuCl2相互作用获得三硫化合物的条件研究","authors":"H. Imanov","doi":"10.18411/ntvesrt-03-2022-07","DOIUrl":null,"url":null,"abstract":"In this study, the conditions for obtaining the compound Cu3(AsS4)2 from the interaction of arsenic(V) sulfide with copper(II) chloride in aqueous medium at a temperature of 323-353 K were studied. The composition of the sample was studied by X-ray phase, differential thermal, thermogravimetric and chemical analysis methods. In contrast to the results of thermogravimetric analysis of the synthesized thio-compound, based on differential thermal and X-ray analysis the obtained compound melts at a temperature of 964.3 K and corresponds to the standard intensity maxima of the Cu3AsS4 compound, respectively.","PeriodicalId":104319,"journal":{"name":"Научные тенденции в эпоху стремительного развития технологий","volume":"372 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Investigation of the conditions for the acquisition of triple thio-compounds from the interaction of As2S5 and CuCl2\",\"authors\":\"H. Imanov\",\"doi\":\"10.18411/ntvesrt-03-2022-07\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, the conditions for obtaining the compound Cu3(AsS4)2 from the interaction of arsenic(V) sulfide with copper(II) chloride in aqueous medium at a temperature of 323-353 K were studied. The composition of the sample was studied by X-ray phase, differential thermal, thermogravimetric and chemical analysis methods. In contrast to the results of thermogravimetric analysis of the synthesized thio-compound, based on differential thermal and X-ray analysis the obtained compound melts at a temperature of 964.3 K and corresponds to the standard intensity maxima of the Cu3AsS4 compound, respectively.\",\"PeriodicalId\":104319,\"journal\":{\"name\":\"Научные тенденции в эпоху стремительного развития технологий\",\"volume\":\"372 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1900-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Научные тенденции в эпоху стремительного развития технологий\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.18411/ntvesrt-03-2022-07\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Научные тенденции в эпоху стремительного развития технологий","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.18411/ntvesrt-03-2022-07","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Investigation of the conditions for the acquisition of triple thio-compounds from the interaction of As2S5 and CuCl2
In this study, the conditions for obtaining the compound Cu3(AsS4)2 from the interaction of arsenic(V) sulfide with copper(II) chloride in aqueous medium at a temperature of 323-353 K were studied. The composition of the sample was studied by X-ray phase, differential thermal, thermogravimetric and chemical analysis methods. In contrast to the results of thermogravimetric analysis of the synthesized thio-compound, based on differential thermal and X-ray analysis the obtained compound melts at a temperature of 964.3 K and corresponds to the standard intensity maxima of the Cu3AsS4 compound, respectively.
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