{"title":"绿色合成氧化镍纳米粒子的紫丁香芳香提取物:表征和生物应用","authors":"S. M. Jassim, M. A. Abd, Israa A. Hammed","doi":"10.55810/2312-5721.1024","DOIUrl":null,"url":null,"abstract":"In this study, nickel oxide (NiO) nanoparticles were successfully synthesized by Syzygium aromaticum (clove) extract via a green synthesis method and evaluated their antibacterial properties. The bio-molecules inside the extract play an important role in converting nickel nitrate salt into nickel oxide nanoparticles. The prepared nickel oxide nanoparticles were characterized via different techniques such as X-ray Diffraction, fourier transform infrared spectroscopy, fi eld emission-scanning electron microscopy and ultraviolet e visible spectrophotometer. From X-ray diffraction results, the crystallite size of NiO NPs was estimated to be (39.7 nm). The fourier transform infrared spectroscopy exhibits intense two peaks at 594 cm ¡ 1 and 469 cm ¡ 1 which indicates the formation of NiO NPs. In addition, the energy band-gap calculated by Tauc ' s formula was ~2.89 eV. Finally, The antibacterial activity study results detected that NiO NPs have the highest activity against Staphylococcus aureus when compared to Escherichia coli . Thus, the present study exhibits good antibacterial activity, which may be explored in future clinical treatments.","PeriodicalId":218143,"journal":{"name":"Al-Bahir Journal for Engineering and Pure Sciences","volume":"133 9 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-04-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Green synthesis of Nickel Oxide Nanoparticles using Syzygium Aromatic Extract: Characterization and Biological Applications\",\"authors\":\"S. M. Jassim, M. A. Abd, Israa A. Hammed\",\"doi\":\"10.55810/2312-5721.1024\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, nickel oxide (NiO) nanoparticles were successfully synthesized by Syzygium aromaticum (clove) extract via a green synthesis method and evaluated their antibacterial properties. The bio-molecules inside the extract play an important role in converting nickel nitrate salt into nickel oxide nanoparticles. The prepared nickel oxide nanoparticles were characterized via different techniques such as X-ray Diffraction, fourier transform infrared spectroscopy, fi eld emission-scanning electron microscopy and ultraviolet e visible spectrophotometer. From X-ray diffraction results, the crystallite size of NiO NPs was estimated to be (39.7 nm). The fourier transform infrared spectroscopy exhibits intense two peaks at 594 cm ¡ 1 and 469 cm ¡ 1 which indicates the formation of NiO NPs. In addition, the energy band-gap calculated by Tauc ' s formula was ~2.89 eV. Finally, The antibacterial activity study results detected that NiO NPs have the highest activity against Staphylococcus aureus when compared to Escherichia coli . Thus, the present study exhibits good antibacterial activity, which may be explored in future clinical treatments.\",\"PeriodicalId\":218143,\"journal\":{\"name\":\"Al-Bahir Journal for Engineering and Pure Sciences\",\"volume\":\"133 9 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-04-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Al-Bahir Journal for Engineering and Pure Sciences\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.55810/2312-5721.1024\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Al-Bahir Journal for Engineering and Pure Sciences","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.55810/2312-5721.1024","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Green synthesis of Nickel Oxide Nanoparticles using Syzygium Aromatic Extract: Characterization and Biological Applications
In this study, nickel oxide (NiO) nanoparticles were successfully synthesized by Syzygium aromaticum (clove) extract via a green synthesis method and evaluated their antibacterial properties. The bio-molecules inside the extract play an important role in converting nickel nitrate salt into nickel oxide nanoparticles. The prepared nickel oxide nanoparticles were characterized via different techniques such as X-ray Diffraction, fourier transform infrared spectroscopy, fi eld emission-scanning electron microscopy and ultraviolet e visible spectrophotometer. From X-ray diffraction results, the crystallite size of NiO NPs was estimated to be (39.7 nm). The fourier transform infrared spectroscopy exhibits intense two peaks at 594 cm ¡ 1 and 469 cm ¡ 1 which indicates the formation of NiO NPs. In addition, the energy band-gap calculated by Tauc ' s formula was ~2.89 eV. Finally, The antibacterial activity study results detected that NiO NPs have the highest activity against Staphylococcus aureus when compared to Escherichia coli . Thus, the present study exhibits good antibacterial activity, which may be explored in future clinical treatments.