水热法制备氧化物(Ga2O3, ZnO, TiO2)及其衍生物纳米颗粒

E. Rusu, V. Morari, T. Guțul, V. Ursaki, P. Vlăzan
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摘要

本文综述了近年来水热法制备氧化纳米颗粒及其衍生物的研究进展。制备了一系列Ga2O3、ZnO和TiO2纳米粒子及其衍生物,包括GaN纳米线和ZnO/TiO2纳米复合材料。以硝酸水合金属为前驱体制备了Ga2O3和ZnO纳米粉体,以异丙醇钛为前驱体制备了TiO2纳米粉体。采用氮化镓纳米材料制备了氮化镓纳米线。用扫描电子显微镜(SEM)、x射线衍射(XRD)和傅里叶变换红外光谱(FTIR)对制备的纳米材料进行了表征。采用光致发光光谱法对掺入Eu3+的Ga2O3纳米粒子进行了表征,以评价其在纳米荧光粉材料中的应用前景。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Hydrothermal preparation of oxide (Ga2O3, ZnO, TiO2) and derivative nanoparticles
A brief review of our recent research on preparation and characterization of oxide nanoparticles and their derivatives by hydrothermal growth is presented. A series of Ga2O3 , ZnO, and TiO2 nanoparticles, as well derivative nanomaterials including GaN nanowires and ZnO/TiO2 nanocompostes have been prepared. Ga2O3 and ZnO nanopowders have been produced using metal nitrate hydrates as precursors, while Titanium isopropoxide was used for preparation of TiO2 nanopowders. GaN nanowires have been produced by nitridation of Ga2O3 nanomaterials. The produced nanomaterials have been characterized scanning electron microscopy (SEM), X-ray diffraction (XRD) analysis and Fourier transform infrared (FTIR) spectroscopy. Ga2O3 nanoparticles doped with Eu3+ ions have been characterized by photoluminescence spectroscopy in order to assess their prospects in developing nanophosphors materials.
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