高银纳米颗粒浆料的分析与烧结优化

D. Michal, M. Janda, J. Řeboun
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引用次数: 0

摘要

本文对新型高银纳米银浆的分析、测试和工艺优化进行了研究。具体来说,在陶瓷基板上印刷导电图案由厚膜技术创建。烧结是目前电力电子领域中最值得期待的一种基板上模具的连接方式。由于陶瓷的多孔结构和陶瓷的特殊属性,特别是在这种情况下使用无压烧结,将陶瓷基板与印刷图案结合使用带来了新的挑战。本文重点分析和比较了新型纳米颗粒浆料与市售银烧结浆料的结构和性能。接下来的步骤是用不同的沉积技术进行初步测试,并制定最佳的烧结轮廓。烧结后还进行了试验。剪切试验显示机械弹性,x射线扫描分析内部结构和立体分析烧结膏体。将温度峰值从45分钟延长至60分钟,并将其温度升高至280℃,所形成的接头效果更好。具有较高的抗剪强度和较均匀的烧结组织。低孔隙率和纳米颗粒的存在显示出更均匀、更稳定、更耐机械分离连接的巨大潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Analysis and Sintering Optimization of Nanoparticle Paste with High Silver Content
This paper deals with analysis, testing, and process optimization of new nanoparticle silvering paste with high silver content. Specifically, on ceramic substrates with printed conductive patterns created by thick film technology. Sintering is currently one of the most anticipated ways of connecting dies on substrates in power electronics field. Using ceramic substrates in combination with printed patterns brings out new challenges because of porous structure and ceramic specific attributes, especially when using presureless sintering as in this case. Presented paper is focused on analysis and comparison of structure and behaviour of the new nanoparticle paste with commercially available silver sintering pastes. Following step was initial testing with different deposition techniques and development of optimal sintering profile. After sintering examinations were also carried out. Shear test showing mechanical resilience, x-ray scanning for analysis of internal structure and stereoscopic analysis of sintered paste. Prolonging the temperature peak from 45 to 60 minutes and rising its temperature to 280°C shows better results in created joint. Higher shear strength was achieved together with more homogenous sintered structure. Lower porosity and presence of nanoparticles shows great potential for more homogenous, stable, and more resistive connection to mechanical separation.
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