直接激光沉积镍基元素粉末原位合成多组分合金

D. Masaylo, S. Igoshin, A. Popovich
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摘要

本文研究了激光熔覆(LC)和直接激光沉积(DLD)制备经典耐热合金的方法。这种方法对应于利用经济上可行的增材技术开发小型金属产品生产的概念。讨论了从纯元素粉末中获得的材料的结果,以及通过3D打印从液相形成合金以及金属基复合材料的发展前景。本文介绍了用Ni / Cr / Fe粉末机械混合形成试样的结果,其主要成分的质量比接近于合金Inconel 600。用光学显微镜和电子显微镜对制备的多层试样进行了研究。测量试样中化学成分的波动,以确定合金中元素的扩散程度。发现沿轨迹边界形成氧化铬团簇,这可能是在熔体结晶过程中沿消热方向扩散。试样的结构表现为大而细长的晶粒,尺寸可达1-2毫米,明显超过一次的高度。晶粒生长方向与试样在Z轴方向上的生长方向相对应。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
IN-SITU SYNTHESIS OF MULTICOMPONENT ALLOYS FROM Ni BASED ELEMENTAL POWDERS BY DIRECT LASER DEPOSITION
The paper investigates an approach to the synthesis of classical heat-resistant alloys by laser cladding (LC) or direct laser deposition (DLD). This approach corresponds to the concept of developing the production of small parties of metal products with the economically feasible use of additive technologies. The results of already obtained materials from pure elemental powders and the prospects for the development of such formation of alloys from the liquid phase, as well as metal-matrix composites by 3D printing, are discussed. The paper presents the result of a specimen formation from a mechanical mixture of Ni / Cr / Fe powder, in the mass ratio of the main components, close in composition to the alloy Inconel 600. The produced multilayer specimen was studied by optical and electron microscopy. Measurement of fluctuations in the chemical composition in the specimen to determine the degree of diffusion of elements in the alloy was carried out. The formation of chromium oxide clusters along the boundaries of the tracks, which, presumably, diffuse in the direction of heat removal during crystallization from the melt, was found. The structure of the specimen is represented by large, elongated grains up to 1-2 mm in size, significantly exceeding the height of one pass. The direction of grain growth corresponds to the growth direction of the specimen in the direction of the Z axis.
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