微机械和化学条件对可切削复合材料粘接的影响

Abdulrahman Abdulrab, A. Attia, Mahy Hassouna
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引用次数: 0

摘要

目的:评价微机械和化学调理对复合陶瓷(可切削复合材料MZ100块)粘接的影响。材料和方法:采用CAD/CAM技术,根据所需尺寸(宽10mm,厚4mm),制造了64个可加工的复合圆盘(MZ100范式)。将圆盘分为两组(n=32):采用Al2O3 (50-μm)研磨组(AM)和喷砂组(SB)。每个主组按化学调理方法又分为常规硅烷(SI)和多用途引物(MP)两个亚组(n=16)。根据所需尺寸(4.5 mm宽x 3.5 mm厚)制作复合树脂盘。将表面处理过的MZ100盘按照粘接性树脂胶结剂、多级粘接性树脂胶结剂和自粘接性树脂胶结剂的类型与复合树脂盘进行粘接。粘接后1小时,所有标本在37℃水浴中保存5个月,然后热循环10000次。经人工时效处理后,所有粘结试件均采用万能Instron试验机进行剪切强度测试。通过双目光学显微镜和扫描电镜对脱粘破坏模式进行了评估。采用3-Way anova进行统计分析。结果:经三因素方差分析,(SB)组与(AM)组SBS差异有统计学意义(p=0.000),不同树脂胶合剂组SBS差异有统计学意义(p=0.006)。而不同化学调理方法间差异无统计学意义(p=0.132)。结论:MZ100型砌块采用自粘或多级粘接树脂胶合剂时,建议对砌块表面进行喷砂处理。与多步粘接树脂水泥相比,各组自粘胶均表现出SBS值。建议对MZ100型块体表面进行微机械和化学调理相结合,而不是单独进行化学调理。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Influence of Micromechanical and Chemical Conditioning on Bonding to Machinable Composite
Purpose: To evaluate the influence of micromechanical and chemical conditioning on bonding to hybrid ceramic (machinable composite MZ100 blocks). Materials and methods: A total of 64 machinable composite discs (MZ100 paradigm) were fabricated using CAD/CAM technology according to the desired dimensions (10 mm width and 4 mm thickness). The discs were divided in two main groups (n=32): as milled group (AM) and sandblast group (SB) used Al2O3 (50-μm). Each main group was subdivided into two subgroups (n=16) according to method of chemical conditioning: conventional silane (SI) and multipurpose primer (MP). Composite resin discs were fabricated according to desired dimensions (4.5 mm width x 3.5 mm thickness). Surface treated MZ100 discs were bonded to the composite resin discs according to the types of adhesive resin cements, multistep adhesive resin cements or self-adhesive resin cements. One hour after bonding, all specimens were stored in water bath at 37°C for 5 months followed by thermocycling for 10,000 cycles. Following artificial aging all bonded specimens underwent shear bond strength testing using universal Instron testing machine. Assessment of the debonding failure mode was done by Binocular optical microscope and SEM. Statistical analysis was performed using a 3-Way ANOVAs.Results: In Three-Way ANOVAs test revealed statistically significant different in SBS between (SB) and (AM) groups {p=0.000} and between different resin cements used {p=0.006}. While there, was no statistically significant different when used different chemical conditioning methods {p=0.132}. Conclusions: Sandblasting of the MZ100 paradigm block surface is recommended when luting with the self-adhesive or multistep adhesive resin cements. The self-adhesive performed SBS values compared to multistep adhesive resin cement in all groups. The combination between micromechanical and chemical conditioning of MZ100 paradigm block surface are recommended over the chemical conditioning alone.
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