阴极电弧蒸发法制备的AlCrN涂层的组织、形貌和力学性能

A. Gilewicz, R. Jȩdrzejewski, P. Myśliński, B. Warcholiński
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引用次数: 0

摘要

利用阴极电弧蒸发在钢基体(HS6-5-2)上形成了CrAlN涂层。研究了氮压力和衬底偏压对Al80Cr20阴极制备的CrAlN涂层性能的影响,包括:涂层的化学成分和物相组成、表面形貌、沉积速率、硬度和与衬底的附着力。结果表明,在压力为3 Pa的氮气气氛中,镀层的沉积速率最高,随着衬底负偏压的增加,镀层的沉积速率降低。涂层表面粗糙度参数Ra随着氮气压力的增大而减小。据推测,这与涂层表面大颗粒数量的减少有关。涂层的硬度(考虑测量不确定度)与氮压力无关,但随着衬底负偏置电压的增加而增加。随着氮气压力的增加,涂层的附着力逐渐增大,然后减小。在涂层形成过程中,衬底负偏置电压的增加使其与衬底的附着力恶化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Structure, morphology and mechanical properties of AlCrN coatings obtained by the method of cathodic arc evaporation
CrAlN coatings have been formed on steel substrates (HS6-5-2) using cathodic arc evaporation. The influence of nitrogen pres-sure and substrate bias voltage on the properties of CrAlN coatings formed from Al80Cr20 cathode, such as: chemical and phase composition of the coatings, their surface morphology, deposition rate, hardness and adhesion to the substrate have been investigated. It has been determined that the rate of the deposition of coatings in the nitrogen atmosphere with the pressure of 3 Pa is the highest and that with the increase of the negative bias voltage of the substrate the deposition rate decreases. The roughness parameter Ra of the coating surface decreases as the nitrogen pressure increases during their formation. Presumably, this is related to the reduction of the amount of macroparticles on the surface of the coating. The hardness of the coatings (taking into account the measurement uncertainty) is independent of the nitrogen pressure, but it increases with the increase of the negative bias voltage of the substrate. The adhesion of the coating increases with the increase of the nitrogen pressure to 3–4 Pa, and then it decreases. The increase in the negative bias voltage of the substrate during the formation of the coating deteriorates its adhesion to the substrate.
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