能量捕获对QCM性能的影响

M. Onoe
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引用次数: 13

摘要

石英晶体微天平(QCM)在厚度剪切模式下振动被广泛应用于生物传感。由于其外围是密封的空气或液密,以形成样品空间,因此为了保持其Q值,从而保持高灵敏度,减少外围位移是很重要的。一种流行的技术是在QCM的中心部分捕获振动能量。通过使中心部分的谐振频率低于外围部分的谐振频率,在厚度剪切模式下实现。当工作频率低于10mhz时,其主要表面通常轮廓为平凸、凸凸或斜角形状。当工作频率高得多时,平坦表面上电极中心部分的简单质量负荷足以引起能量捕获。然而,能量捕获减少了传感的有效面积,从而降低了QCM的总体灵敏度。在分析了能量捕获对QCM性能影响的基础上,一个好的QCM设计需要在这两个因素之间取得平衡。将以往基于自由主面轮廓振子等效电路的分析扩展到考虑被测介质对主面机械载荷的影响。针对振动器的小截面,设计了一种新的四端口等效电路。两个端口对应于振动器的上下表面,端接待测介质的机械阻抗。另外两个端口,左和右,用于与相邻部分连接。等效电路的参数取决于截面的厚度或质量载荷。大量具有逐渐变化的厚度或质量载荷的截面串联在一起,以近似振动器的轮廓。将补偿定理应用于整体等效电路,表明传感器的灵敏度与位移幅度的平方积分成正比。计算了平面-凸振子的谐振频率、位移分布和灵敏度折减系数作为宽度与厚度比和宽度与曲率半径的函数
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Effect of energy trapping on performance of QCM
Quartz crystal microbalance (QCM) vibrating in a thickness shear mode is widely used for biosensing. Since its peripheral is sealed air or liquid tight to form a sample space, a reduction of displacement at peripheral is important in order to keep its Q value and hence its sensitivity high. A popular technique is a trapping of vibration energy in the center portion of QCM. It is realized in the thickness shear mode by making the resonant frequency of the center portion lower than the resonant frequency of the peripheral. When an operating frequency is below 10 MHz, its major surfaces are usually contoured in either plano-convex, convex-convex or bevel shape. When an operating frequency is much higher, simple mass loading by electrodes in the center portion on flat surfaces is good enough to cause energy trapping. Energy trapping, however, reduces an effective area for sensing and hence an overall sensitivity of QCM. A good design of QCM calls for a balance between two factors based on an analysis of effect of energy trapping on performance of QCM. Previous analysis based on equivalent circuit of contoured vibrators with free major surfaces is extended to include effects of mechanical loading on major surfaces due to medium to be sensed into account. A new equivalent circuit with four ports is developed for small section of a vibrator. Two ports correspond to upper and lower surfaces of the vibrator and are terminated by mechanical impedance of attached media to be sensed. Another two ports, left and right, are for connection with neighboring sections. Parameters of an equivalent circuit depend on thickness or mass loading of a section. A large number of sections with gradually varying thickness or mass loading are connected in tandem to approximate a profile of the vibrator. An application of the compensation theorem to the overall equivalent circuit shows the sensor sensitivity is proportional to the integral of square of displacement amplitude. Resonant frequencies, distribution of displacement and reduction factor of sensitivity of plano-convex vibrators are calculated as functions of width vs. thickness ratio and width vs. radius of curvature
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