{"title":"碱化处理:NaOH浓度对复合材料苎麻纤维性能的改善","authors":"U. Jamilah, S. Sujito","doi":"10.17146/jsmi.2021.22.3.6182","DOIUrl":null,"url":null,"abstract":"THE IMPROVEMENT OF RAMIE FIBER PROPERTIES AS COMPOSITE MATERIALS USING ALKALIZATION TREATMENT: NaOH CONCENTRATION. Ramie fiber is a plant fiber that has good quality and potential as a constituent of composite materials. In this study, ramie fiber surface modification was conducted through alkalization with various at 0%, 4%, 5%, 6%, 7%, 8%, and 9% concentrations of NaOH using a magnetic stirrer with a speed of 200 rpm at 70οC for 5 hours. Alkaline ramie fibers are characterized using the Cheson method to determine the chemical composition of ramie fiber, FT-IR test to determine the function group of ramie fiber, morphological test to know the surface structure and diameter of ramie fiber, as well as tensile test to know the tensile strength and tensile modulus of PLA/ramie composite. Overall, the increase of NaOH concentration up to 8% percentage was able to increase the level of cellulose and lignin ramie fibers by 88.180 % and 2.444 %, as well as lower hemicellulose levels of 1.446 %. The alkalization treatment of 8% NaOH, optimally reduces the hydrophilic properties of the fiber. The increased concentration of NaOH makes the fiber surface cleaner and the diameter smaller, but the fiber structure is damaged at a concentration of NaOH more than 8%. Tensile test results showed that alkalized ramie fibers with an 8% concentration of NaOH produced PLA/ramie composites with the highest tensile strength and tensile modulus of 57.37 MPa and 248.25 MPa. Thus, the optimum ramie fiber properties are increased using alkalization with an 8% concentration of NaOH.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"56 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"THE IMPROVEMENT OF RAMIE FIBER PROPERTIES AS COMPOSITE MATERIALS USING ALKALIZATION TREATMENT: NaOH CONCENTRATION\",\"authors\":\"U. Jamilah, S. Sujito\",\"doi\":\"10.17146/jsmi.2021.22.3.6182\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"THE IMPROVEMENT OF RAMIE FIBER PROPERTIES AS COMPOSITE MATERIALS USING ALKALIZATION TREATMENT: NaOH CONCENTRATION. Ramie fiber is a plant fiber that has good quality and potential as a constituent of composite materials. In this study, ramie fiber surface modification was conducted through alkalization with various at 0%, 4%, 5%, 6%, 7%, 8%, and 9% concentrations of NaOH using a magnetic stirrer with a speed of 200 rpm at 70οC for 5 hours. Alkaline ramie fibers are characterized using the Cheson method to determine the chemical composition of ramie fiber, FT-IR test to determine the function group of ramie fiber, morphological test to know the surface structure and diameter of ramie fiber, as well as tensile test to know the tensile strength and tensile modulus of PLA/ramie composite. Overall, the increase of NaOH concentration up to 8% percentage was able to increase the level of cellulose and lignin ramie fibers by 88.180 % and 2.444 %, as well as lower hemicellulose levels of 1.446 %. The alkalization treatment of 8% NaOH, optimally reduces the hydrophilic properties of the fiber. The increased concentration of NaOH makes the fiber surface cleaner and the diameter smaller, but the fiber structure is damaged at a concentration of NaOH more than 8%. Tensile test results showed that alkalized ramie fibers with an 8% concentration of NaOH produced PLA/ramie composites with the highest tensile strength and tensile modulus of 57.37 MPa and 248.25 MPa. Thus, the optimum ramie fiber properties are increased using alkalization with an 8% concentration of NaOH.\",\"PeriodicalId\":365391,\"journal\":{\"name\":\"Jurnal Sains Materi Indonesia\",\"volume\":\"56 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1900-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Jurnal Sains Materi Indonesia\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.17146/jsmi.2021.22.3.6182\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Jurnal Sains Materi Indonesia","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17146/jsmi.2021.22.3.6182","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 5
摘要
碱化处理:NaOH浓度对复合材料苎麻纤维性能的改善。苎麻纤维是一种具有优良品质和潜力的植物纤维,可作为复合材料的组成部分。在本研究中,苎麻纤维的表面改性是通过在0%、4%、5%、6%、7%、8%和9%的NaOH浓度下,在磁力搅拌器上进行碱化,转速为200转/分,温度为70 o o,时间为5小时。对碱性苎麻纤维进行表征,采用Cheson法测定苎麻纤维的化学成分,FT-IR法测定苎麻纤维的功能基团,形态学试验了解苎麻纤维的表面结构和直径,拉伸试验了解PLA/苎麻复合材料的拉伸强度和拉伸模量。结果表明,当NaOH浓度增加8%时,纤维素和木质素含量分别提高了88.180%和2.444%,半纤维素含量降低了1.446%。碱化处理为8% NaOH,最大限度地降低了纤维的亲水性。NaOH浓度的增加使纤维表面更清洁,纤维直径变小,但NaOH浓度超过8%时纤维结构被破坏。拉伸试验结果表明,在NaOH浓度为8%的情况下,碱化苎麻纤维得到的PLA/苎麻复合材料的拉伸强度和拉伸模量最高,分别为57.37 MPa和248.25 MPa。因此,使用浓度为8%的NaOH碱化可以提高苎麻纤维的最佳性能。
THE IMPROVEMENT OF RAMIE FIBER PROPERTIES AS COMPOSITE MATERIALS USING ALKALIZATION TREATMENT: NaOH CONCENTRATION
THE IMPROVEMENT OF RAMIE FIBER PROPERTIES AS COMPOSITE MATERIALS USING ALKALIZATION TREATMENT: NaOH CONCENTRATION. Ramie fiber is a plant fiber that has good quality and potential as a constituent of composite materials. In this study, ramie fiber surface modification was conducted through alkalization with various at 0%, 4%, 5%, 6%, 7%, 8%, and 9% concentrations of NaOH using a magnetic stirrer with a speed of 200 rpm at 70οC for 5 hours. Alkaline ramie fibers are characterized using the Cheson method to determine the chemical composition of ramie fiber, FT-IR test to determine the function group of ramie fiber, morphological test to know the surface structure and diameter of ramie fiber, as well as tensile test to know the tensile strength and tensile modulus of PLA/ramie composite. Overall, the increase of NaOH concentration up to 8% percentage was able to increase the level of cellulose and lignin ramie fibers by 88.180 % and 2.444 %, as well as lower hemicellulose levels of 1.446 %. The alkalization treatment of 8% NaOH, optimally reduces the hydrophilic properties of the fiber. The increased concentration of NaOH makes the fiber surface cleaner and the diameter smaller, but the fiber structure is damaged at a concentration of NaOH more than 8%. Tensile test results showed that alkalized ramie fibers with an 8% concentration of NaOH produced PLA/ramie composites with the highest tensile strength and tensile modulus of 57.37 MPa and 248.25 MPa. Thus, the optimum ramie fiber properties are increased using alkalization with an 8% concentration of NaOH.