提取介质和酸类型对柑桔皮分离果胶理化性质的影响

Hager A. Abd- Elazize, E. H. Rahma, T. El-Adawy, A. E. Elbltagy
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引用次数: 0

摘要

果胶作为添加剂广泛应用于食品、医药和化妆品行业。本研究以柑桔皮为原料生产果胶,研究提取介质类型和提取浓度对柑桔皮分离果胶理化性质的影响,以及以柑桔皮为原料提取果胶的不同影响因素。柠檬酸和盐酸的果胶收率分别为54.80%和23.44%。结果表明,柠檬酸和盐酸的最佳提取浓度分别为1 N和0.3N,提取时间和温度分别为60 min和90℃。提取果胶所用的酸不同,分离得到的果胶理化性质也有显著差异。柠檬酸处理的果胶中灰分和水分含量低于盐酸处理。温度对其理化性质如当量质量、甲氧基含量、总无水醛酸等有显著影响,但对酯化程度影响不显著。本研究得到的果胶具有高甲氧基果胶(HMP)的特征,因为DE高于50%。两种酸的总无水醛酸含量均低于65%,因此分离出的果胶需进一步纯化。结果表明,柠檬酸法制备的果胶具有较好的理化性能,是评价果胶质量的良好指标。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
EFFECT OF EXTRACTION MEDIUM AND ACID TYPE ON THE PHYSIO -CHEMICAL PROPERTIES OF ORANGE PEELS ISOLATED PECTIN
Pectin is found to be widely used as additives in food, pharmaceutical and cosmetic industries. This study was carried out using orange peel as raw material to produce pectin and studied the effect of extraction medium type and concentrations on the Physio -chemical properties of orange peels isolated pectin and the different factors affecting pectin extraction and characterization using orange peel as raw material. Citric acid was higher in pectin yield 54.80% and 23.44% using citric and Hcl respectively. The optimum acid concentrations for pectin extraction was found to be 1 N and 0.3N for citric and Hcl respectively and the suitable time and temperature for extraction was 60 min and 90 o c for both acids used. There was a significant difference in isolated pectin physiochemical properties according to the acid used for pectin extraction. The contents of ash and a moisture in isolated pectins were lower for citric acid compared to Hcl treatment. Temperature had a significant effect on some Physio -chemical properties such as equivalent weight, methoxyl content and total anhydrouronic acid but degree of esterification wasn't significantly affected. Pectin's obtained in this study were characterized as high methoxyl pectin (HMP) since the DE was higher than 50 %. Total anhydrouronic acid for both acid was low than 65% so the pectin isolated needs more purification. In general results proved that orange citric acid prepared pectin has better physio -chemical properties which are a good indications in pectin quality evaluation.
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