希夫碱包覆银纳米粒子作为污水中铅的吸附剂。

49 Pub Date : 2023-06-30 DOI:10.56714/bjrs.49.1.4
Ahmed M. Zaidan, Zainab T. Alabdullah, Uhood J. Al-Hamdani
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引用次数: 0

摘要

合成了包覆席夫碱的纳米银。用希夫碱还原和涂覆银纳米粒子。希夫碱起到封盖作用,防止氧化银过度生长。希夫碱生产的纳米银具有新颖的形状和独特的外观。席夫碱作为还原和封盖剂的存在使制备的银纳米颗粒具有新的形状。利用光谱数据(1h核磁共振(H1NMR)、质谱和傅里叶变换红外光谱(FTIR))分析了希夫碱的结构。用紫外可见光谱法观察了461 nm表面等离子体带内银纳米粒子的形成。在扫描电子显微镜图像中可以看到球形和粒径在50到100纳米之间的银纳米颗粒。首次使用包裹有席夫碱的银纳米颗粒吸附污染水中的铅。吸附率为69%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Silver nanoparticles coated by Schiff base as an adsorbent of lead from polluted water.
Synthesis of silver nanoparticles coated with Schiff base was achieved . Silver nanoparticles are reduced and coated using Schiff base. Schiff base serves as a capping to stop silver oxide from overgrowing. Schiff base produces silver nanoparticles with a novel form and a distinctive appearance. The presence of Schiff base as a reducing and capping agent can give a new shape for prepared silver nanoparticles. The structure of Schiff base was analyzed based on spectral data (1 H nuclear magnetic resonance (H1NMR), Mass spectroscopy, and Fourier-transform infrared spectroscopy (FTIR). The formation of silver nanoparticles within a surface plasmon band at 461 nm was observed using UV-Vis Spectroscopy. Silver nanoparticles with a spherical shape and a particle size between 50 and 100 nm are visible in a scanning electron microscope image. For the first time, silver nanoparticles coated with Schiff base were used to adsorb lead from a sample of polluted water. The rate of adsorption was 69%.
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49
49
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