Production of WE43 magnesium alloy by powder metallurgy and the effect of glucose on wear resistance in biocorrosive wear.

IF 1.6 4区 医学 Q4 BIOPHYSICS
Biointerphases Pub Date : 2023-03-01 DOI:10.1116/6.0002270
Bünyamin Çiçek
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引用次数: 0

Abstract

In this study, WE43 magnesium alloy was produced by the powder metallurgy method. Microstructural analyses of the produced samples were carried out using the scanning electron microscopy method. X-ray fluorescence, energy dispersive x-ray (EDS) analysis, and hardness tests were also implemented to investigate the physical and chemical properties of the alloys. The volumetric hardness was measured to be approximately 53 HV. The microstructural analysis and EDS results indicated the presence of Mg24Y5 and Mg41Nd5 phases in the alloys. Reciprocating-type experiments were carried out in dry and corrosive environments to evaluate the wear resistance. Hanks's solution containing 2% g/l glucose was used as the corrosive environment. Gluconic acid resulting from the oxidation of glucose in the Hanks's solution formed a new thin layer on the alloy surface, which was observed in the worn surface images. The formation of the thin film on the alloy surface resulted in an increase in wear resistance by 37%. The results unraveled the potential of the WE43 alloys as implant materials in areas in contact with glucose.

粉末冶金法制备WE43镁合金及葡萄糖对生物腐蚀磨损耐磨性的影响
本研究采用粉末冶金法制备了WE43镁合金。用扫描电子显微镜对制备的样品进行了显微结构分析。采用x射线荧光、能谱分析(EDS)和硬度测试对合金的理化性能进行了研究。测量的体积硬度约为53 HV。显微组织分析和能谱分析表明,合金中存在Mg24Y5和Mg41Nd5相。在干燥和腐蚀环境下进行往复式试验,评价其耐磨性。采用含2% g/l葡萄糖的Hanks溶液作为腐蚀环境。在汉克斯溶液中葡萄糖氧化产生的葡萄糖酸在合金表面形成了一层新的薄层,这在磨损表面图像中可以观察到。在合金表面形成薄膜后,其耐磨性提高了37%。结果揭示了WE43合金在与葡萄糖接触区域作为植入材料的潜力。
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来源期刊
Biointerphases
Biointerphases 生物-材料科学:生物材料
自引率
0.00%
发文量
35
期刊介绍: Biointerphases emphasizes quantitative characterization of biomaterials and biological interfaces. As an interdisciplinary journal, a strong foundation of chemistry, physics, biology, engineering, theory, and/or modelling is incorporated into originated articles, reviews, and opinionated essays. In addition to regular submissions, the journal regularly features In Focus sections, targeted on specific topics and edited by experts in the field. Biointerphases is an international journal with excellence in scientific peer-review. Biointerphases is indexed in PubMed and the Science Citation Index (Clarivate Analytics). Accepted papers appear online immediately after proof processing and are uploaded to key citation sources daily. The journal is based on a mixed subscription and open-access model: Typically, authors can publish without any page charges but if the authors wish to publish open access, they can do so for a modest fee. Topics include: bio-surface modification nano-bio interface protein-surface interactions cell-surface interactions in vivo and in vitro systems biofilms / biofouling biosensors / biodiagnostics bio on a chip coatings interface spectroscopy biotribology / biorheology molecular recognition ambient diagnostic methods interface modelling adhesion phenomena.
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