Physical and acoustical performance of natural rubber foam prepared via microwave and convection heating techniques

IF 1.2 4区 化学 Q4 POLYMER SCIENCE
Nur Syuhada Ahmad Zauzi, Zulkifli Mohamad Ariff, Raa Khimi Shuib, Mohd Fadzil Ain
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Abstract

Conventional manufacturing techniques of natural rubber foam (NRF) require long processing time besides producing closed cell structure, a property that limits the application of the NRF. The NRF produced via compression moulding (CPM) and microwave-convection oven heating techniques were compared in this study. The correlation between different processing techniques with the physical, morphological, and acoustic properties of NRF was examined. The results indicated that in all the processing techniques, an increase in the blowing agent (BA) led to a decrease in the density of the NRF. Heating the material sequentially with 16 parts per hundred (phr) of BA in a microwave oven at 1000 Watts, and then, in a convection oven at 150 ℃ produced NRF with a density of 0.23 g/cm3. In contrast, the NRF produced by CPM with 16 phr of BA had a density of 0.35 g/cm3. Scanning electron microscope analysis revealed that the NRF generated by CPM had fewer interconnected and more closed cells. On the other hand, sequential heating using microwave and convection heating techniques and vice versa led to the production of NRF with more open and interconnected cells. The prepared NRF was examined for acoustic properties. The results showed that the NRF produced by CPM at 12 and 16 phr of BA had the lowest ability to attenuate sound wave energy. This was due to the highly solid surface of the sample, which caused high sound wave reflection. Open and interconnected cells significantly improved the acoustic efficiency. These findings indicated that microwave-assisted heating techniques can modify the cellular structure of NRF and produce the material within a shorter period.

Abstract Image

Abstract Image

通过微波和对流加热技术制备的天然橡胶泡沫的物理和声学性能
天然橡胶泡沫(NRF)的传统制造技术除了产生闭孔结构外,还需要较长的加工时间,这一特性限制了 NRF 的应用。本研究比较了通过压缩成型(CPM)和微波对流炉加热技术生产的天然橡胶泡沫。研究了不同加工技术与 NRF 的物理、形态和声学特性之间的相关性。结果表明,在所有加工技术中,发泡剂(BA)的增加都会导致 NRF 密度的降低。在 1000 瓦特的微波炉中依次加热百万分之 16 (phr) 的发泡剂,然后在 150 ℃ 的对流炉中加热,生产出的 NRF 密度为 0.23 g/cm3。相比之下,用 16 短语 BA 的 CPM 生产的 NRF 密度为 0.35 克/立方厘米。扫描电子显微镜分析表明,CPM 生成的 NRF 具有更少的相互连接和更多的闭合细胞。另一方面,使用微波和对流加热技术进行顺序加热(反之亦然)可生成具有更多开放和相互连接细胞的 NRF。对制备的 NRF 进行了声学特性检测。结果表明,CPM 在 12 和 16 phr 的 BA 下制备的 NRF 衰减声波能量的能力最低。这是由于样品表面高度坚固,导致声波反射率较高。而开放式和相互连接的单元则大大提高了声学效率。这些研究结果表明,微波辅助加热技术可以改变 NRF 的细胞结构,并在更短的时间内生产出材料。
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来源期刊
Journal of Rubber Research
Journal of Rubber Research 化学-高分子科学
自引率
15.40%
发文量
46
审稿时长
3 months
期刊介绍: The Journal of Rubber Research is devoted to both natural and synthetic rubbers, as well as to related disciplines. The scope of the journal encompasses all aspects of rubber from the core disciplines of biology, physics and chemistry, as well as economics. As a specialised field, rubber science includes within its niche a vast potential of innovative and value-added research areas yet to be explored. This peer reviewed publication focuses on the results of active experimental research and authoritative reviews on all aspects of rubber science. The Journal of Rubber Research welcomes research on: the upstream, including crop management, crop improvement and protection, and biotechnology; the midstream, including processing and effluent management; the downstream, including rubber engineering and product design, advanced rubber technology, latex science and technology, and chemistry and materials exploratory; economics, including the economics of rubber production, consumption, and market analysis. The Journal of Rubber Research serves to build a collective knowledge base while communicating information and validating the quality of research within the discipline, and bringing together work from experts in rubber science and related disciplines. Scientists in both academia and industry involved in researching and working with all aspects of rubber will find this journal to be both source of information and a gateway for their own publications.
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