The Effect of 3-aminopropyltrimethyoxysilane (AMEO) as a Coupling Agent on Curing and Mechanical Properties of Natural Rubber/Palm Kernel Shell Powder Composites

Procedia Chemistry Pub Date : 2016-01-01 DOI:10.1016/j.proche.2016.03.019

Shuhairiah Daud, Hanafi Ismail, Azhar Abu Bakar

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引用次数: 13

Abstract

This research is conducted using palm kernel shell powder (PKS) as filler in natural rubber The effect of 3-aminopropyltrimethoxysilane as coupling agent on composites were studied at different palm kernel shell loading i.e, 0 5, 10, 15 and 20 phr The palm kernel shell was crushed and sieved to an average particle size of 5.53 μm The palm kernel shell filled natural rubber composites were prepared using laboratory size two roll mill The curing characteristics such as scorch time, cure time and maximum torque were obtained from rheometer The palm kernel shell powder filled natural rubber composites were cured at 150^oC using hot press according to their cure time Curing characteristics, tensile properties, rubber-filler interaction and morphological properties of palm kernel shell powder filled natural rubber were studied Scorch time and cure time show reduction but tensile strength, elongation at break, modulus at 100% (M100) and modulus at 300% (M300) increased with the presence of 3-aminopropyltrimethyloxysilane Rubber-filler interaction studies showed that rubber filler interaction in natural rubber filled with palm kernel shell powder improved with incorporation of 3-aminopropyltrimethyoxysilane.

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偶联剂3-氨基丙基三甲基氧基硅烷(AMEO)对天然橡胶/棕榈仁壳粉复合材料固化及力学性能的影响

进行本研究使用棕榈仁贝壳粉(PKS)作为填料在天然橡胶3-aminopropyltrimethoxysilane作为偶联剂对复合材料的影响研究在不同的棕榈仁壳加载即0 5、10、15和20 phr棕榈仁壳压碎,已筛平均粒径为5.53μm棕榈仁壳填充天然橡胶复合材料准备使用实验室规模两辊轧机固化特征如烧焦时间,研究了棕榈仁壳粉填充天然橡胶复合材料的固化时间、固化特性、拉伸性能、橡胶与填料的相互作用以及棕榈仁壳粉填充天然橡胶的形态性能。橡胶与填料的相互作用研究表明，加入3-氨基丙基三甲基氧基硅烷后，棕榈仁壳粉填充的天然橡胶中橡胶填料的相互作用得到改善。

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Procedia Chemistry

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