Investigation on synthesis of two ammonium based ionic liquids from fatty acids and triethylamine

T. T. Bui, T. Dang, Khun Borin, Thanh Nam Ly, Trung T. Pham, Thanh Xuan Thi Phan, Ngoc Pham-Cong
{"title":"Investigation on synthesis of two ammonium based ionic liquids from fatty acids and triethylamine","authors":"T. T. Bui, T. Dang, Khun Borin, Thanh Nam Ly, Trung T. Pham, Thanh Xuan Thi Phan, Ngoc Pham-Cong","doi":"10.51316/jca.2023.012","DOIUrl":null,"url":null,"abstract":"Two ionic liquids triethylammonium oleate and  triethylammonium stearate were synthesized from fatty acids and triethyl amine using two different methods (one step and three step methods). The yield triethylammonium oleate rearch 68.8-74% (one step method) and 86.3% (three step method) and of triethylammonium stearate rearch 68.7-74.1 (one step method) and 83.5% (three step method). The one step method spends more time but less chemicals and brings higher yield. FT-IR and 1H-NMR spectra of ILs obtained from both method was measured. The results showed that synthesis method doesn’t affect on the structure of the products and ILs obtained from one step method has higher purity.","PeriodicalId":23507,"journal":{"name":"Vietnam Journal of Catalysis and Adsorption","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2023-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Vietnam Journal of Catalysis and Adsorption","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.51316/jca.2023.012","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

Abstract

Two ionic liquids triethylammonium oleate and  triethylammonium stearate were synthesized from fatty acids and triethyl amine using two different methods (one step and three step methods). The yield triethylammonium oleate rearch 68.8-74% (one step method) and 86.3% (three step method) and of triethylammonium stearate rearch 68.7-74.1 (one step method) and 83.5% (three step method). The one step method spends more time but less chemicals and brings higher yield. FT-IR and 1H-NMR spectra of ILs obtained from both method was measured. The results showed that synthesis method doesn’t affect on the structure of the products and ILs obtained from one step method has higher purity.
脂肪酸和三乙胺合成两种铵基离子液体的研究
以脂肪酸和三乙胺为原料,采用一步法和三步法合成了油酸三乙胺和硬脂酸三乙胺两种离子液体。油酸三乙铵的收率分别为68.8-74%(一步法)和86.3%(三步法),硬脂酸三乙铵的收率分别为68.7-74.1(一步法)和83.5%(三步法)。一步走法耗时多,化学药品少,产量高。测定了两种方法得到的红外光谱和核磁共振光谱。结果表明,合成方法对产物的结构没有影响,一步法得到的il具有较高的纯度。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 求助全文
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信