{"title":"Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction","authors":"C. Pilapong, T. Thongtem, S. Thongtem","doi":"10.1109/INEC.2010.5425105","DOIUrl":null,"url":null,"abstract":"Spikes of Sb<inf>2</inf>S<inf>3</inf> (antimony sulfide) were synthesized by hydrothermal reaction at 100–200 °C for 6–48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb<inf>2</inf>S<inf>3</inf> in the shape of spikes, with their growths in the [001] direction and E<inf>g</inf> of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment.","PeriodicalId":6390,"journal":{"name":"2010 3rd International Nanoelectronics Conference (INEC)","volume":"53 1","pages":"558-559"},"PeriodicalIF":0.0000,"publicationDate":"2010-03-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"2010 3rd International Nanoelectronics Conference (INEC)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/INEC.2010.5425105","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100–200 °C for 6–48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb2S3 in the shape of spikes, with their growths in the [001] direction and Eg of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment.
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