V. Bongiovanni, M. Colombo, A. Cavallero, D. Talarico
{"title":"Determining Odor-Active Compounds in a Commercial Sample ofCinnamomum cassia Essential Oil Using GC-MS and GC-O","authors":"V. Bongiovanni, M. Colombo, A. Cavallero, D. Talarico","doi":"10.4172/2157-7064.1000347","DOIUrl":null,"url":null,"abstract":"The volatiles of a commercial sample of Cinnamomum cassia (Nees and T. Nees) J. Presl. essential oil were analyzed by gas chromatography-mass spectrometry (GC-MS). The identification of the components was confirmed by Kovats retention index and their quantities were established using internal standard. These analyses had led to the identification of 72 chemicals and quantification of 41 of them. The majority of volatiles identified belongs to oxygenated compounds (e.g., aldehydes) while non oxygenated terpenes represent about 18% of the oil. The odor quality of cassia essential oil was assessed by Gas Chromatography-Olfactometry (GC-O). Among the 26 components identified with GC-O, AEDA (Aroma Extract Dilution Analysis) has allowed to establish a number of components with high dilution factor (strongly odorous) such as cinnamaldehyde, 3-phenylpropanal, guaiacol and 2-phenylethanol.","PeriodicalId":15534,"journal":{"name":"Journal of Chromatography & Separation Techniques","volume":"85 1","pages":"1-7"},"PeriodicalIF":0.0000,"publicationDate":"2017-01-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Chromatography & Separation Techniques","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.4172/2157-7064.1000347","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 5
Abstract
The volatiles of a commercial sample of Cinnamomum cassia (Nees and T. Nees) J. Presl. essential oil were analyzed by gas chromatography-mass spectrometry (GC-MS). The identification of the components was confirmed by Kovats retention index and their quantities were established using internal standard. These analyses had led to the identification of 72 chemicals and quantification of 41 of them. The majority of volatiles identified belongs to oxygenated compounds (e.g., aldehydes) while non oxygenated terpenes represent about 18% of the oil. The odor quality of cassia essential oil was assessed by Gas Chromatography-Olfactometry (GC-O). Among the 26 components identified with GC-O, AEDA (Aroma Extract Dilution Analysis) has allowed to establish a number of components with high dilution factor (strongly odorous) such as cinnamaldehyde, 3-phenylpropanal, guaiacol and 2-phenylethanol.
肉桂(Nees and T. Nees)商业样品的挥发物。采用气相色谱-质谱联用技术(GC-MS)对精油进行分析。采用科瓦茨保留指数进行鉴定,并采用内标法确定其含量。这些分析鉴定出72种化学物质,并对其中41种进行了定量分析。鉴定出的大部分挥发物属于含氧化合物(例如醛),而非含氧萜约占油的18%。采用气相色谱-嗅觉法(GC-O)评价决明子精油的气味品质。在GC-O鉴定的26种成分中,AEDA(香气提取稀释分析)允许建立一些具有高稀释系数(强烈气味)的成分,如肉桂醛,3-苯丙醛,愈创木酚和2-苯乙醇。