NiO/ZnO Core-Shell Nanoparticles In Situ Synthesis Via Microemulsion Method

D. Han, C. Wang, D. Li, Z. Cao
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引用次数: 10

Abstract

Nanoparticles of NiO(core)/ZnO(shell) core-shell and nanoparticles were successfully prepared in Triton X-100/n-hexanol/cyclohexane/water W/O microemulsion system. Basic synthesis conditions were determined. Ni(OH)2/Zn(OH)2 nanoparticles were first synthesized at room temperature then calcined at 500°C to form NiO/ZnO nanoparticles. The calcined products were studied by means of TEM, and XRD analyzers. The mechanism of the core shell NiO/ZnO nanoparticles formation is explained.
微乳液法原位合成NiO/ZnO核壳纳米颗粒
在Triton X-100/正己醇/环己烷/水W/O微乳液体系中成功制备了NiO(核)/ZnO(壳)核-壳和纳米颗粒。确定了基本合成条件。首先在室温下合成Ni(OH)2/Zn(OH)2纳米颗粒,然后在500℃下煅烧得到NiO/ZnO纳米颗粒。采用透射电镜(TEM)和x射线衍射仪(XRD)对煅烧产物进行了研究。阐述了核壳型NiO/ZnO纳米颗粒的形成机理。
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