STUDY OF THE EFFECT OF SOLVENT AND QUANTITY OF CATALYST ON ARICRYL POLYMERIZATION AT PT. ARISTEK HIGHPOLYMER BEKASI

N. H. Airun, Zukhrufi Zukhrufi, F. I. Fajarwati
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Abstract

Aricryl synthesis was carried out by feeding technique. The monomers used were styrene, isobutyl acrylate, 2-HEMA and acrylamide powder. The catalysts used were AIBN (Azobisisobutyronitrile) and Perbutyl O98. The synthesis results were then devided by 2 for resin batch G-0915 A was diluted in > 63% mixture of n-butanol and methanol, while for G-0915 B was carried out dilution in > 63% toluene. the results obtained were compared based on the influence of the solvent using the parameters of viscosity, NV/total solid, AV (Acid Value), color and OH value. It was found that the best solvent according to specifications is toluene solvent with a viscosity of Z2-15. The Aricryl batch G-0915 was compared with Aricryl batch G-0903 based on the influence of the quantity of catalyst. The results showed that the increasing quantity of catalyst affects the aging process. Aging duration for Aricryl batch G-0903 was 11 hours, while for Arycril batch G-0915 was 8 hours.
溶剂和催化剂用量对羊尾草高聚物聚合的影响研究
采用进料法合成芳基。所使用的单体有苯乙烯、丙烯酸异丁酯、2-HEMA和丙烯酰胺粉末。催化剂为AIBN(偶氮二异丁腈)和过丁基O98。树脂批G-0915 A在> 63%的正丁醇和甲醇混合物中稀释,G-0915 B在> 63%的甲苯中稀释,合成结果除以2。通过粘度、NV/total solid、AV (Acid Value)、颜色、OH值等参数,比较了溶剂对所得结果的影响。结果表明,符合规格要求的最佳溶剂为粘度为Z2-15的甲苯溶剂。根据催化剂用量的影响,对G-0915和G-0903两批aricyl进行了比较。结果表明,催化剂用量的增加会影响其老化过程。芳烯醇G-0903批次的老化时间为11小时,而芳烯醇G-0915批次的老化时间为8小时。
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