Inoculation Treatment of an Additively Manufactured 2024 Aluminium Alloy with Titanium Nanoparticles

Qiyang Tan, Jingqi Zhang, Qiang Sun, Z. Fan, Gan Li, Yu Yin, Yingang Liu, Mingxing Zhang
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引用次数: 186

Abstract

Abstract Considerable studies on metal selective laser melting (SLM) have proved the necessity to refine microstructure parts fabricated by SLM in order to eliminate property anisotropy, hot-tearing and to increase the SLM-processability. In the present work, Ti nanoparticles, at the first time, were discovered to be an extremely effective inoculant for an SLMed 2024 aluminium alloy. 0.7 wt% addition of Ti nanoparticles was capable of substantially eliminating the hot-tearing cracks and columnar structure, and refining the grains in the SLMed 2024 alloy in a broad processing window. The substantial grain refinement in the Ti-inoculated 2024 alloy was attributed to the in-situ formation of Al3Ti nanoparticles with a L12 ordered structure, which formed a coherent interface with Al matrix and therefore significantly promoted the heterogeneous nucleation of the α-Al during solidification of melt pools in the SLM process. After a conventional T6 heat treatment, this SLMed alloy exhibited a superior balance of strength and ductility (tensile strength was up to 432 ± 20 MPa and elongation of 10 ± 0.8%), which was comparable to its wrought counterpart. This work can be considered as a breakthrough in research of fabricating high-strength aluminium alloys using SLM.
纳米钛孕育处理增材制备2024铝合金
对金属选择性激光熔化(SLM)的大量研究表明,为了消除性能各向异性、热撕裂和提高SLM加工性能,有必要对SLM制造的微结构零件进行细化。在本研究中,Ti纳米颗粒首次被发现是一种非常有效的SLMed 2024铝合金孕育剂。掺量为0.7 wt%的Ti纳米颗粒能够在较宽的加工窗口内消除SLMed 2024合金的热撕裂裂纹和柱状组织,细化晶粒。在SLM过程中,原位形成了具有L12有序结构的Al3Ti纳米颗粒,与Al基体形成共格界面,从而显著促进了α-Al在熔池凝固过程中的非均相形核。经过常规的T6热处理后,该SLMed合金表现出良好的强度和延展性平衡(抗拉强度高达432±20 MPa,伸长率为10±0.8%),与变形后的合金相当。这一研究成果是利用SLM制备高强度铝合金研究的一个突破。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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