PENGARUH KEPADATAN TERNA DAN LAMA PENYULINGAN TERHADAP RENDEMEN DAN KARAKTERISTIK MINYAK Melaleuca bracteata

Nanan Nurdjannah
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Abstract

The influence of material bulk density and duration of distillation on the yi eld and characteristic of Melaleuca bracteata oilMelaleuca bracteata belongs to Myrtaceae family which is grown wildly in Australia and Quensland. The oil is produced from Ihe leaves and (wigs by distillation and is used in fragrances industry. The oil content of leaves and twigs range between 0.4 to 1.0% with metil eugenol as the major component (70-80%). Because of its high metil eugenol content M. bracteata oil can be used to control fruil flies The experiment was carried out to evaluate the influence of material bulk density in the distillation vessel and duration of distillation on the yield and charac¬ teristic of the oil produced. Material used was (he leaves and twigs of M bracteata from the experimental garden of the Research Institute for Spice and Medicinal Crops. Manoko, Lembang (1200 in above the sea level). The experiment at 1993 was designed as completely randomized design, arranged factorially with three replications. The result showed that the optimum distillation condition was 1 56 g/l material bulk density in the vessel and 3 hours distillation. Such distillation condition produced 1.09 % oil yield with (he characteristics as follow speciic gravity I 0263, refractive index 1 5296, optical rotation -3.3°, solubility in 70% cthanol 1 : 1, methyl eugenol content 86.1%, acid number 0.56, ester number 15.4 and ester number after acetylation 39.3. Referring to Australia oil, the Indonesian M bracteata oil has higher value of esther number both before and after acetylation.
物料容重和蒸馏时间对苞片千层油产量和特性的影响苞片千层属桃金娘科,在澳大利亚和昆士兰地区广泛生长。这种油是通过蒸馏从叶子和假发中提取出来的,用于香料工业。叶、枝含油量在0.4 ~ 1.0%之间,以金属丁香酚为主要成分(70 ~ 80%)。由于小苞叶精油中金属丁香酚含量高,可用于防治蝇类。本实验研究了蒸馏容器内物料容重和蒸馏时间对油收率和油特性的影响。所用材料为香料和药用作物研究所实验园的M . brteata的叶子和树枝。兰邦的马诺科(海拔1200米)。1993年试验采用完全随机设计,按因子安排,3个重复。结果表明,最佳蒸馏条件为1 56 g/l,蒸馏时间为3 h。该蒸馏条件下的油收率为1.09%,其特点是:比重为1.0263,折射率为1 5296,旋光度为-3.3°,在70%乙醇中溶解度为1:1,甲基丁香酚含量为86.1%,酸值0.56,酯值15.4,乙酰化后酯值39.3。与澳大利亚油相比,印尼小苞叶油乙酰化前后的esther number值都更高。
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