The Determination of the Water Content in Cigarette Smoke Condensate Using a Karl Fischer Titrator / Wasserbestimmung im Rauchkondensat nach Karl Fischer mit einer halbautomatischen Apparatur
{"title":"The Determination of the Water Content in Cigarette Smoke Condensate Using a Karl Fischer Titrator / Wasserbestimmung im Rauchkondensat nach Karl Fischer mit einer halbautomatischen Apparatur","authors":"H. Buser","doi":"10.2478/CTTR-2013-0194","DOIUrl":null,"url":null,"abstract":"Abstract The current method of determination of the water content of cigarette smoke condensate was improved by using a Karl Fischer titrator with automatic end-point stop. The overall procedure thus becomes faster (the titration time is less than 2 minutes), easier (no supervision is needed during the titration) and better reproducible (coefficient of variation 2.5 % on the amount of water determined). In these three criterions, the automated Karl Fischer method is superior to a gas-chromatographic procedure having served as a method of comparison.","PeriodicalId":35431,"journal":{"name":"Beitrage zur Tabakforschung International/ Contributions to Tobacco Research","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"1968-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Beitrage zur Tabakforschung International/ Contributions to Tobacco Research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2478/CTTR-2013-0194","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Agricultural and Biological Sciences","Score":null,"Total":0}
引用次数: 1
Abstract
Abstract The current method of determination of the water content of cigarette smoke condensate was improved by using a Karl Fischer titrator with automatic end-point stop. The overall procedure thus becomes faster (the titration time is less than 2 minutes), easier (no supervision is needed during the titration) and better reproducible (coefficient of variation 2.5 % on the amount of water determined). In these three criterions, the automated Karl Fischer method is superior to a gas-chromatographic procedure having served as a method of comparison.