Study of Boron Complexation with Pyridoxine: Effect of Interaction Time, Temperature, and Amount of Pyridoxine

N. Hidayati, Ariqah Fianti, Mita Arnela
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Abstract

Borax is one of the compounds of boron (B), which is widely used as an anti-fungal, wood preservative, and antiseptic in cosmetics. Boron can form complexes with biomolecules such as pyridoxine, so it is interesting to know the interaction between borax and pyridoxine. This study seeks to investigate the complexation of boron, which is obtained from borax, with pyridoxine under various conditions of time, temperature, and the amount of pyridoxine. The resulting complex was characterized by UV-Vis spectrophotometry, Fourier Transform Infrared (FT-IR), and X-Ray diffraction (XRD). The study was initiated by optimizing the complexation of boron and pyridoxine. The maximum wavelengths of pyridoxine were found in the 205 nm and 292 nm regions, while the boron-pyridoxine complex was found in the 237 nm region. The obtained contact time, temperature, and amount of pyridoxine are 40 minutes, 60 °C, and 2 mL respectively. The results of the Fourier transform infrared (FT-IR) analysis of the boron-pyridoxine complex showed that there were OH groups, aromatic C=C groups, aliphatic C-C groups, B-H groups, and B-O groups. The results of the XRD analysis of the boron-pyridoxine complex obtained a diffraction angle of 30.93°
硼与吡哆醇络合的研究:作用时间、温度和吡哆醇用量的影响
硼砂是硼(B)的一种化合物,广泛用作抗真菌剂、木材防腐剂和化妆品防腐剂。硼可以与吡哆醇等生物分子形成配合物,因此了解硼砂与吡哆醇的相互作用是很有趣的。本文研究了硼砂制得的硼与吡哆醇在不同时间、温度和吡哆醇用量条件下的络合反应。用紫外-可见分光光度法、傅里叶变换红外光谱(FT-IR)和x射线衍射(XRD)对所得配合物进行了表征。本研究以优化硼与吡哆醇的络合为出发点。吡哆醇的最大波长在205 nm和292 nm,硼-吡哆醇配合物的最大波长在237 nm。得到的接触时间为40分钟,温度为60℃,吡哆醇用量为2 mL。傅里叶变换红外(FT-IR)分析结果表明,硼-吡哆醇配合物中存在OH、芳香C=C、脂肪族C-C、B-H和B-O基团。硼-吡哆醇配合物的XRD分析结果为衍射角为30.93°
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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