Composition and thermal stability of traditional Tibetan mineral medicine Nanhanshuishi

Quan Zhengxiang
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引用次数: 1

Abstract

OBJECTIVE: To determine the composition, structure, trace elements and thermal stability of Tibetan medicine Nanhanshuishi. METHOD: The trace elements, the structure, and the thermal stability of Nanhanshuishi were assayed and calculated by X-ray fluorescence spectrometry (XRF), inductively coupled plasma optical emission spectrometer (ICP-OES), atomic fluorescence spectrometry (AFS), inductively coupled plasma mass spectrometry (ICP-MS), X-ray power diffraction (XRD), TG-DTA. RESULT: The results indicated that the phase is mainly made up of CaCO3 (Rhombohedral, R-3c) in Nanhanshuishi. The analysis of elements show that Nanhanshuishi is rich in Ca and O, and contains other more than 20 minor elements, such as Si, Mg, Fe, Al, Na, K, Zn, Mn, Pb, As, Hg etc. The result of TG-DTA show that the weight of Nanhanshuishi starts to decline from near 700 degrees C and get steady above 850 degrees C. CONCLUSION: The study provided scientific data for the establishment of quality standards of Tibetan medicine Nanhanshuishi.
藏药南寒水石的组成及热稳定性研究
目的:测定藏药南寒水石的组成、结构、微量元素及热稳定性。方法:采用x射线荧光光谱法(XRF)、电感耦合等离子体光学发射光谱仪(ICP-OES)、原子荧光光谱法(AFS)、电感耦合等离子体质谱法(ICP-MS)、x射线功率衍射仪(XRD)、TG-DTA对南寒水石的微量元素、结构和热稳定性进行测定和计算。结果:南汉水石的相主要由CaCO3 (Rhombohedral, R-3c)组成。元素分析表明,南汉水石富含Ca和O,并含有Si、Mg、Fe、Al、Na、K、Zn、Mn、Pb、as、Hg等20多种微量元素。TG-DTA结果表明,在700℃附近,南寒水石的质量开始下降,在850℃以上趋于稳定。结论:本研究为藏药南寒水石质量标准的制定提供了科学依据。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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