Preparation and Characterization of Dextrin in Xanthosoma sagittifolium (L.) Schott Starch with Acid Catalyst and Enzymatic Methods

Sumaiyah, Selvia Wiliantari, Karsono
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Abstract

Abstract. Taro produces carbohydrate. It has the potential as a substitute material for wheat and rice or as diversification into food and raw materials for pharmaceutical industrial. The aim of this study is to prepare and characterize dextrin in Xanthosoma sagittifolium starch with acid catalyst and enzymatic methods. Xanthosoma sagittifolium was mashed and decanted with distilled water. Dextrin was made by acid catalyst method using HCl 1 N and enzymatic method using α-amylase enzyme. Dextrin was characterized and tested according to the Indonesian National Standard (SNI) 01-2593-1992. The results showed that the yield from acid catalyst and enzymatic methods are 41.73 % and 67.10 %, respectively. The color test showed that dextrin from acid catalyst method is yellowish whereas the enzymatic method gives white dextrin. The qualitative test with lugol solution gives brownish purple dextrin. The characteristic of 80 mesh fineness for dextrin fabricated by acid and enzymatic methods are 94.7 % ± 0.06 and 93.96 % ± 0.02 respectively. Dextrin obtained from acid catalyst has higher water content (8.79 % ± 0.15) than dextrin from enzymatic methods (7.62 % ± 0.23) as well as dextrin from acid catalyst has higher the ash content (0.45 % ± 0.02) than dextrin from enzymatic method (0.42 % ± 0.04). Dextrin made from enzymatic method has higher solubility in cold water (63.09 % + 0.1) than dextrin from acid catalyst method (57.47 % ± 0.25). Dextrose equivalent for dextrin produced is 13.65 ± 0.36 and 15.31 ± 0.46 for acid catalyst and enzymatic methods. Melting points for dextrin obtained from acid catalyst and enzymatic methods are 185 oC ± 0.57 and 182 cC ± 0.57 respectively. Acidity degree of dextrin fabricated from acid catalyst and enzymatic methods are 2.86 ± 0.23 and 4.39 ± 0.4. The research shows that the characterization of dextrin by acid catalyst and enzymatic methods meet the quality requirements for Indonesia National Standard (SNI) 01-2593-1992.   Key words: Taro, dextrin, acid catalyst method, enzymatic method
矢状叶黄豆中糊精的制备与表征酸催化和酶促法制备肖特淀粉
摘要芋头产生碳水化合物。它具有作为小麦和大米的替代材料或作为食品和制药工业原料的多样化的潜力。采用酸催化和酶催化法制备了矢叶黄原淀粉中的糊精,并对其进行了表征。将矢状叶黄松捣碎,用蒸馏水倒出。采用盐酸酸催化法和α-淀粉酶法制备糊精。根据印尼国家标准(SNI) 01-2593-1992对糊精进行了表征和检测。结果表明,酸催化法和酶法的产率分别为41.73%和67.10%。颜色试验表明,酸催化法得到的糊精呈淡黄色,酶促法得到的糊精呈白色。用lugol溶液定性试验得到棕紫色糊精。酸法和酶法制备糊精的80目细度特征值分别为94.7%±0.06和93.96%±0.02。酸催化制得的糊精含水量(8.79%±0.15)高于酶法制得的糊精(7.62%±0.23),灰分含量(0.45%±0.02)高于酶法制得的糊精(0.42%±0.04)。酶法制得的糊精在冷水中的溶解度(63.09% + 0.1)高于酸催化法制得的糊精(57.47%±0.25)。酸催化法和酶促法生产的糊精的葡萄糖当量分别为13.65±0.36和15.31±0.46。酸催化法和酶法得到的糊精熔点分别为185℃±0.57和182 cC±0.57。酸催化法和酶法制备的糊精酸度分别为2.86±0.23和4.39±0.4。研究表明,酸催化和酶法表征的糊精符合印尼国家标准(SNI) 01-2593-1992的质量要求。关键词:芋头;糊精;酸催化法
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