Green Synthesis of ZnO Nanoparticles via Sol-gel Method and Investigation of Its Application in Solvent-free Synthesis of 12-Aryl-tetrahydrobenzo[α]xanthene-11-one Derivatives Under Microwave Irradiation

IF 3.5 Q2 CHEMISTRY, MULTIDISCIPLINARY
Saeid Taghavi Fardood, A. Ramazani, Farzaneh Moradnia, Z. Afshari, Sara Ganjkhanlu, F. Zare
{"title":"Green Synthesis of ZnO Nanoparticles via Sol-gel Method and Investigation of Its Application in Solvent-free Synthesis of 12-Aryl-tetrahydrobenzo[α]xanthene-11-one Derivatives Under Microwave Irradiation","authors":"Saeid Taghavi Fardood, A. Ramazani, Farzaneh Moradnia, Z. Afshari, Sara Ganjkhanlu, F. Zare","doi":"10.33945/SAMI/CHEMM.2019.6.2","DOIUrl":null,"url":null,"abstract":"In this work, zinc oxide (ZnO) nanoparticles were fabricated using Arabic gum as a reducing and stabilizing agent by the novel sol-gel method without adding any surfactants. The synthesized nanoparticles were characterized by Fourier transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), and scanning electron microscopy (SEM). Subsequently, ZnO nanoparticles as efficient catalysts were consumed for the three-component coupling of 2-naphthol, aldehydes, and dimedone under microwave irradiation and solvent-free conditions in order to furnish the corresponding synthesis of 12-aryl-tetrahydrobenzo[α]xanthene-11-one derivatives in high yields.","PeriodicalId":9896,"journal":{"name":"Chemical Methodologies","volume":null,"pages":null},"PeriodicalIF":3.5000,"publicationDate":"2019-08-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"28","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemical Methodologies","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.33945/SAMI/CHEMM.2019.6.2","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 28

Abstract

In this work, zinc oxide (ZnO) nanoparticles were fabricated using Arabic gum as a reducing and stabilizing agent by the novel sol-gel method without adding any surfactants. The synthesized nanoparticles were characterized by Fourier transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), and scanning electron microscopy (SEM). Subsequently, ZnO nanoparticles as efficient catalysts were consumed for the three-component coupling of 2-naphthol, aldehydes, and dimedone under microwave irradiation and solvent-free conditions in order to furnish the corresponding synthesis of 12-aryl-tetrahydrobenzo[α]xanthene-11-one derivatives in high yields.
溶胶-凝胶法绿色合成纳米ZnO及其在微波辐射下无溶剂合成12-芳基四氢苯并[α]杂蒽-11- 1衍生物中的应用研究
在不添加任何表面活性剂的情况下,以阿拉伯胶为还原剂和稳定剂,采用溶胶-凝胶法制备了氧化锌纳米颗粒。采用傅里叶变换红外光谱(FTIR)、粉末x射线衍射(XRD)和扫描电镜(SEM)对合成的纳米颗粒进行了表征。随后,利用ZnO纳米颗粒作为高效催化剂,在微波辐射和无溶剂条件下进行了2-萘酚、醛和二美酮的三组分偶联,从而高收率地合成了相应的12-芳基四氢苯并[α]杂蒽-11- 1衍生物。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 求助全文
来源期刊
Chemical Methodologies
Chemical Methodologies CHEMISTRY, MULTIDISCIPLINARY-
CiteScore
3.10
自引率
1.80%
发文量
8
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信