Effect of the Fuel in the Synthesis of NiO–YSZ by Solution Combustion Synthesis with Potential Application in Catalysis of Hydrogen

IF 0.5 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY
A. A. Lopera, E. A. Chavarriaga, J. A. Perez-Taborda, S. L. Amaya, A. Echavarría, C. García
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引用次数: 1

Abstract

Nanocomposites of nickel oxide/yttria-stabilized zirconia (NiO/YSZ) particles were synthesized via solution combustion synthesis using glycine and urea as fuels in one step. The powders were characterized by X-ray diffraction (XRD) analysis, where the synthesis with urea showed the formation of the NiO/YSZ composite, while the presence of Ni with NiO/YSZ were observed when the glycine was used. The morphology of the as-prepared powders and the presence of Ni were corroborated by field emission scanning electron microscopy and energy dispersive X-ray spectroscopy (FE-SEM; EDX). The powders showed catalytic behavior which was evidenced by H2-TPR measurements. These materials could be used for the fabrication of Ni/YSZ anode for fuel cells.

Abstract Image

燃料对溶液燃烧合成NiO-YSZ的影响及其在氢催化方面的潜在应用
以甘氨酸和尿素为燃料,采用溶液燃烧法一步合成了氧化镍/氧化钇稳定氧化锆(NiO/YSZ)纳米复合材料。用x射线衍射(XRD)对粉末进行了表征,其中尿素合成时形成了NiO/YSZ复合材料,而甘氨酸合成时发现NiO/YSZ中存在Ni。通过场发射扫描电镜和能量色散x射线能谱(FE-SEM)对制备的粉末的形貌和Ni的存在进行了证实;EDX)。H2-TPR测试证实了粉末的催化性能。这些材料可用于制备燃料电池用Ni/YSZ阳极。
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来源期刊
CiteScore
1.00
自引率
33.30%
发文量
27
期刊介绍: International Journal of Self-Propagating High-Temperature Synthesis  is an international journal covering a wide range of topics concerned with self-propagating high-temperature synthesis (SHS), the process for the production of advanced materials based on solid-state combustion utilizing internally generated chemical energy. Subjects range from the fundamentals of SHS processes, chemistry and technology of SHS products and advanced materials to problems concerned with related fields, such as the kinetics and thermodynamics of high-temperature chemical reactions, combustion theory, macroscopic kinetics of nonisothermic processes, etc. The journal is intended to provide a wide-ranging exchange of research results and a better understanding of developmental and innovative trends in SHS science and applications.
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