A. A. Lopera, E. A. Chavarriaga, J. A. Perez-Taborda, S. L. Amaya, A. Echavarría, C. García
{"title":"Effect of the Fuel in the Synthesis of NiO–YSZ by Solution Combustion Synthesis with Potential Application in Catalysis of Hydrogen","authors":"A. A. Lopera, E. A. Chavarriaga, J. A. Perez-Taborda, S. L. Amaya, A. Echavarría, C. García","doi":"10.3103/S1061386222020042","DOIUrl":null,"url":null,"abstract":"<p>Nanocomposites of nickel oxide/yttria-stabilized zirconia (NiO/YSZ) particles were synthesized via solution combustion synthesis using glycine and urea as fuels in one step. The powders were characterized by X-ray diffraction (XRD) analysis, where the synthesis with urea showed the formation of the NiO/YSZ composite, while the presence of Ni with NiO/YSZ were observed when the glycine was used. The morphology of the as-prepared powders and the presence of Ni were corroborated by field emission scanning electron microscopy and energy dispersive X-ray spectroscopy (FE-SEM; EDX). The powders showed catalytic behavior which was evidenced by H<sub>2</sub>-TPR measurements. These materials could be used for the fabrication of Ni/YSZ anode for fuel cells.</p>","PeriodicalId":595,"journal":{"name":"International Journal of Self-Propagating High-Temperature Synthesis","volume":null,"pages":null},"PeriodicalIF":0.5000,"publicationDate":"2022-06-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Self-Propagating High-Temperature Synthesis","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.3103/S1061386222020042","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 1
Abstract
Nanocomposites of nickel oxide/yttria-stabilized zirconia (NiO/YSZ) particles were synthesized via solution combustion synthesis using glycine and urea as fuels in one step. The powders were characterized by X-ray diffraction (XRD) analysis, where the synthesis with urea showed the formation of the NiO/YSZ composite, while the presence of Ni with NiO/YSZ were observed when the glycine was used. The morphology of the as-prepared powders and the presence of Ni were corroborated by field emission scanning electron microscopy and energy dispersive X-ray spectroscopy (FE-SEM; EDX). The powders showed catalytic behavior which was evidenced by H2-TPR measurements. These materials could be used for the fabrication of Ni/YSZ anode for fuel cells.
期刊介绍:
International Journal of Self-Propagating High-Temperature Synthesis is an international journal covering a wide range of topics concerned with self-propagating high-temperature synthesis (SHS), the process for the production of advanced materials based on solid-state combustion utilizing internally generated chemical energy. Subjects range from the fundamentals of SHS processes, chemistry and technology of SHS products and advanced materials to problems concerned with related fields, such as the kinetics and thermodynamics of high-temperature chemical reactions, combustion theory, macroscopic kinetics of nonisothermic processes, etc. The journal is intended to provide a wide-ranging exchange of research results and a better understanding of developmental and innovative trends in SHS science and applications.