Processability and Microstructural Evolution of W360 Hot Work Tool Steel by Directed Energy Deposition

IF 3.3 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Josip Vinčić, Alberta Aversa, Mariangela Lombardi, Diego Manfredi
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Abstract

Laser directed energy deposition (L-DED) was used to produce samples of the newly patented W360 hot work tool steel by Böhler. The process parameters were optimized to obtain nearly fully dense samples through the production and analysis of single deposited tracks and single layers. Subsequently, bulk samples underwent a hardening heat treatment, consisting of austenitizing, air quenching, and tempering. The samples were analysed in the as-built condition (AB), after quenching (Q) and following tempering cycles (HT) to observe the microstructural evolution. The microstructure was investigated using optical and scanning electron microscopes, energy dispersive X-ray analysis, and X-ray diffraction analysis. Furthermore, the microstructural evolution was analysed with differential scanning calorimetry, while the mechanical response was evaluated through microhardness test. It was found that the AB samples exhibited a dendritic-cellular microstructure with tempered martensite laths. The thermal history of the AB samples was completely modified by the austenitizing treatment followed by quenching, resulting in a fully martensitic Q sample that did not display the typical dendritic-cellular microstructure of the L-DED process. The completion of the heat treatment with tempering cycles revealed the presence of Mo-rich carbides dispersed in a martensitic matrix. The HT samples exhibited a mean microhardness of 634 HV, remaining constant along the entire building direction from the substrate to the last deposited layer, indicating a homogeneous microstructure. This high value, similar to other hot work tool steels such as H13, makes W360 a very promising candidate for tool build and repair purposes.

Graphical Abstract

Abstract Image

W360热作工具钢定向能量沉积工艺性能及组织演变
激光定向能量沉积(L-DED)被用于生产博勒最新获得专利的 W360 热作工具钢样品。通过生产和分析单个沉积轨迹和单层,对工艺参数进行了优化,以获得几乎完全致密的样品。随后,批量样品进行了硬化热处理,包括奥氏体化、空气淬火和回火。对样品的坯料状态(AB)、淬火后(Q)和回火循环(HT)进行分析,以观察微观结构的演变。使用光学和扫描电子显微镜、能量色散 X 射线分析和 X 射线衍射分析对微观结构进行了研究。此外,还使用差示扫描量热法分析了微观结构的演变,并通过显微硬度测试评估了机械响应。结果发现,AB 样品呈现出树枝状细胞微观结构,并带有回火马氏体板条。通过奥氏体化处理后的淬火,AB 样品的热历史被完全改变,形成了完全马氏体化的 Q 样品,没有显示出 L-DED 工艺中典型的树枝状细胞微观结构。完成回火循环热处理后,马氏体基体中出现了富钼碳化物。HT 样品的平均显微硬度为 634 HV,从基体到最后沉积层的整个构建方向上保持恒定,这表明微观结构是均匀的。这一高数值与其他热作工具钢(如 H13)相似,使 W360 成为一种非常有前途的工具制造和维修候选材料。
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来源期刊
Metals and Materials International
Metals and Materials International 工程技术-材料科学:综合
CiteScore
7.10
自引率
8.60%
发文量
197
审稿时长
3.7 months
期刊介绍: Metals and Materials International publishes original papers and occasional critical reviews on all aspects of research and technology in materials engineering: physical metallurgy, materials science, and processing of metals and other materials. Emphasis is placed on those aspects of the science of materials that are concerned with the relationships among the processing, structure and properties (mechanical, chemical, electrical, electrochemical, magnetic and optical) of materials. Aspects of processing include the melting, casting, and fabrication with the thermodynamics, kinetics and modeling.
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