Selective laser sintering of acrylonitrile butadiene styrene polymer and post-processing enhancement: an experimental study

IF 2.4 3区 化学 Q3 POLYMER SCIENCE
Chen Jibing, Chen Junsheng, Yang Junsheng, Wu Yiping
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Abstract

Acrylonitrile butadiene styrene (ABS) polymer refers to a high-molecular-weight amorphous copolymer with a wide softening range and specific viscoelasticity of polymer material. The application of such powder materials in additive manufacturing technology for selective laser sintering (SLS) for forming and its post-processing enhancement are rarely investigated. In this paper, the standard specimens of ABS powder were fabricated by SLS. The dimensional accuracy and the mechanical properties of specimens were examined, and the microstructure of tensile fracture was observed under a scanning electron microscope (SEM). The tensile, flexural, and impact strengths were obtained as 2.44 MPa, 5.10 MPa, and 2.77 kJ/m2, respectively, as indicated by the results of this study. Accordingly, the SLS ABS parts are not suitable as functional prototypes. According to the thermodynamic equation, dissolution equation, capillary permeability formula, and the selection of diluent, the influence of diluent on viscosity, the influence of curing time on viscosity, and the influence of curing agent and viscosity on permeability are studied. Thus, the parts were infiltrated with two different types of epoxy resin (system Y and system W) to enhance the mechanical properties. The mechanical properties of specimens administrated with curing agent W increased 4.57, 3.87, and 1.64 times in terms of tensile, flexural, and impact strength, respectively; the others administrated with curing agent Y increased 6.38, 3.52, and 1.05 times, respectively. Accordingly, the results indicate that the SLS ABS parts enhanced by epoxy resin can serve as function parts, which is a feasible method since the properties of the composites can be readily tailored by changing different infiltration resins.

Graphical abstract

Abstract Image

选择性激光烧结丙烯腈-丁二烯-苯乙烯聚合物及其后处理强化的实验研究
丙烯腈-丁二烯-苯乙烯(ABS)聚合物是指高分子量的无定形共聚物,具有较宽的软化范围和聚合物材料的特定粘弹性。这种粉末材料在选择性激光烧结(SLS)增材制造技术中的应用及其后处理增强很少被研究。本文采用SLS法制备了ABS粉末的标准试样。检测了试样的尺寸精度和力学性能,并在扫描电子显微镜(SEM)下观察了拉伸断裂的微观结构。如本研究结果所示,拉伸强度、弯曲强度和冲击强度分别为2.44MPa、5.10MPa和2.77kJ/m2。因此,SLS ABS零件不适合作为功能原型。根据热力学方程、溶解方程、毛细管渗透率公式和稀释剂的选择,研究了稀释剂对粘度的影响、固化时间对粘度的作用以及固化剂和粘度对渗透率的影响。因此,用两种不同类型的环氧树脂(系统Y和系统W)渗透零件以提高机械性能。在拉伸、弯曲和冲击强度方面,加入固化剂W的试样的力学性能分别提高了4.57、3.87和1.64倍;其他给药固化剂Y的剂量分别增加了6.38倍、3.52倍和1.05倍。因此,结果表明,环氧树脂增强的SLS ABS零件可以作为功能零件,这是一种可行的方法,因为通过改变不同的渗透树脂可以很容易地调整复合材料的性能。图形摘要
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来源期刊
Iranian Polymer Journal
Iranian Polymer Journal 化学-高分子科学
CiteScore
4.90
自引率
9.70%
发文量
107
审稿时长
2.8 months
期刊介绍: Iranian Polymer Journal, a monthly peer-reviewed international journal, provides a continuous forum for the dissemination of the original research and latest advances made in science and technology of polymers, covering diverse areas of polymer synthesis, characterization, polymer physics, rubber, plastics and composites, processing and engineering, biopolymers, drug delivery systems and natural polymers to meet specific applications. Also contributions from nano-related fields are regarded especially important for its versatility in modern scientific development.
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