Simultaneous measurements of the two-dimensional distribution of infrared laser intensity and temperature in a single-sided laser-heated diamond anvil cell

Abstract

In this report, we demonstrate that combining the laser heating system in a diamond anvil cell (LH-DAC) with a tandem acoustic-optical tunable filter (LH-DAC–TAOTF) allows for the simultaneous measurement of (a) the relative infrared (IR, 1070 nm) power distribution on a specimen surface in the DAC; (b) the temperature distribution under laser heating of a specimen under high-pressure in a DAC; it also (c) provides an opportunity to control the shape of the IR laser spot on the surface of the heated specimen. The effect of the π-shaper on the shape and the position of the focus of the IR laser beam on a specimen using a TAOTF is also presented. For a 10× long-working distance objective, the smallest diameter of the IR laser was found to be around 10 μm, when the focal plane coincides with that of the imaging optical system of LH-DAC. The highest diameter of the IR laser was shown to be 20 μm when the rim of the π-shaper was set at 3 μm. It is demonstrated also that the TAOFT not only permits to measure the two-dimensional (2-D) distribution of the IR laser power, but also allows for the alignment of the laser before each heating event at different pressures.