Optimization of ultrasound-assisted extraction of polyphenols from globe artichoke (Cynara scolymus L.) bracts residues using response surface methodology.

IF 1.3 Q4 FOOD SCIENCE & TECHNOLOGY

Acta scientiarum polonorum. Technologia alimentaria Pub Date : 2021-07-01 DOI:10.17306/J.AFS.0937

Miguel Angel Quispe, José Alberto Pacheco Valenzuela, Alex Rubén Huamán de la Cruz, Clara Raquel Espinoza Silva, Greta Hinostroza Quiñonez, Galia Mavel Manyari Cervantes

{"title":"Optimization of ultrasound-assisted extraction of polyphenols from globe artichoke (Cynara scolymus L.) bracts residues using response surface methodology.","authors":"Miguel Angel Quispe, José Alberto Pacheco Valenzuela, Alex Rubén Huamán de la Cruz, Clara Raquel Espinoza Silva, Greta Hinostroza Quiñonez, Galia Mavel Manyari Cervantes","doi":"10.17306/J.AFS.0937","DOIUrl":null,"url":null,"abstract":"Background: The globe artichoke (Cynara scolymus L.) is a rich source of phenolic compounds which may be extracted by ultrasound technology and used as a medicinal alternative. The objective of this work was to determine the radiation amplitude (%), ethanol concentration (%), and time extraction (min) required to guarantee an elevated content of polyphenol compounds.Methods: The optimal extraction conditions were assessed through the Box-Wilson design and by applying Composite Face Centered (CCFC) and total phenolic compounds (TPC) as the response variables.Results: A quadratic model was adequate, with R2 = 0.993. The optimal conditions were a radiation amplitude of 97%, an ethanol concentration of 53%, and an extraction time of 9.7 min. The optimized extract of artichoke bracts (Cynara scolymus L.) showed a TPC of 25.13 (±0.030) mg GAE/g, an antioxidant activity DPPH of 39.79 (±0.014) mmol Trolox equivalents (TE), and an antioxidant capacity TEAC of 33.98 (±0.03) mmol Trolox equivalents.Conclusions: The results showed values closely related to the expected values, indicating that the models were well-developed.","PeriodicalId":7209,"journal":{"name":"Acta scientiarum polonorum. Technologia alimentaria","volume":"20 3","pages":"277-290"},"PeriodicalIF":1.3000,"publicationDate":"2021-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta scientiarum polonorum. Technologia alimentaria","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17306/J.AFS.0937","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"FOOD SCIENCE & TECHNOLOGY","Score":null,"Total":0}

引用次数: 3

Abstract

Background: The globe artichoke (Cynara scolymus L.) is a rich source of phenolic compounds which may be extracted by ultrasound technology and used as a medicinal alternative. The objective of this work was to determine the radiation amplitude (%), ethanol concentration (%), and time extraction (min) required to guarantee an elevated content of polyphenol compounds.

Methods: The optimal extraction conditions were assessed through the Box-Wilson design and by applying Composite Face Centered (CCFC) and total phenolic compounds (TPC) as the response variables.

Results: A quadratic model was adequate, with R2 = 0.993. The optimal conditions were a radiation amplitude of 97%, an ethanol concentration of 53%, and an extraction time of 9.7 min. The optimized extract of artichoke bracts (Cynara scolymus L.) showed a TPC of 25.13 (±0.030) mg GAE/g, an antioxidant activity DPPH of 39.79 (±0.014) mmol Trolox equivalents (TE), and an antioxidant capacity TEAC of 33.98 (±0.03) mmol Trolox equivalents.

Conclusions: The results showed values closely related to the expected values, indicating that the models were well-developed.

查看原文本刊更多论文

响应面法优化超声辅助提取洋蓟叶残渣中多酚的工艺条件。

背景:洋蓟(Cynara scolymus L.)是一种富含酚类化合物的植物，可通过超声技术提取并作为药用替代品。本工作的目的是确定辐射幅度(%)、乙醇浓度(%)和提取时间(min)，以保证多酚化合物的含量升高。方法:采用Box-Wilson设计，以复合面心(CCFC)和总酚类化合物(TPC)为响应变量，评价最佳提取条件。结果:二次型模型成立，R2 = 0.993。最佳提取条件为辐射强度97%、乙醇浓度53%、提取时间9.7 min。优化后的洋蓟叶提取物TPC为25.13(±0.030)mg GAE/g，抗氧化活性DPPH为39.79(±0.014)mmol Trolox当量(TE)，抗氧化能力TEAC为33.98(±0.03)mmol Trolox当量。结论:所得结果与期望值密切相关，表明所建立的模型是完善的。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

求助全文

约1分钟内获得全文求助全文

来源期刊

Acta scientiarum polonorum. Technologia alimentaria FOOD SCIENCE & TECHNOLOGY-

CiteScore

2.70

自引率

0.00%

发文量