Revealing the deformation behavior and microstructure evolution in Mg-12Y–1Al alloy during hot compression

IF 6.3 2区 材料科学 Q2 CHEMISTRY, PHYSICAL
Shuai Yuan , Jinhui Wang , Lei Zhang , Peipeng Jin
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引用次数: 2

Abstract

In this study, the hot uniaxial compression of the heat-treated Mg-12Y–1Al alloy containing long-period stacking ordered (LPSO) phase was conducted by a Gleeble-3500 simulator. Compressive mechanical properties at elevated temperatures and the effects of deformation temperature (300–450 ℃) and strain rate (0.001–1 s−1) on the hot deformation behavior of the alloy were systematically investigated. Combining with an optical microscope (OM), electron backscatter diffraction (EBSD), and in-grain misorientation axes (IGMA) analysis, the microstructure and texture evolution, dislocation slip, and dynamic recrystallization (DRX) mechanism of the alloy was studied in detail. The results showed that the flow stress decreased with the increase in temperature and the decrease in strain rate. At a strain rate of 1 s−1, the compressive strength at 300 ℃ and 350 ℃ was basically the same. After deformation, the morphology of Al2Y had almost no change, while the LPSO underwent apparent kinking deformation. The increase in temperature was conducive to DRX. The DRX mechanism of the alloy mainly included discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX), and DDRX was dominant. The dense lamellar LPSO at the grain boundary was detrimental to the occurrence of DDRX. In addition, the deformed microstructure presented a typical [0001]//CD (compression direction) texture. With the increase in temperature, the texture intensity decreased progressively due to the activation of multiple slip systems and the increased DRX fraction. At a strain rate of 0.01 s−1, when the temperature increased to 450 ℃, the number of deformed grains dominated by pyramidal Ⅱ<c+a> slip increased substantially.

揭示了Mg-12Y-1Al合金在热压缩过程中的变形行为和组织演变
本研究采用Gleeble-3500模拟装置对含长周期有序堆积相(LPSO)的热处理Mg-12Y-1Al合金进行了热单轴压缩实验。系统研究了高温压缩力学性能、变形温度(300 ~ 450℃)和应变速率(0.001 ~ 1 s−1)对合金热变形行为的影响。结合光学显微镜(OM)、电子背散射衍射(EBSD)和晶内错取向轴(IGMA)分析,对合金的显微组织和织构演化、位错滑移和动态再结晶(DRX)机理进行了详细研究。结果表明,流变应力随温度的升高和应变速率的减小而减小。在应变速率为1 s−1时,300℃和350℃的抗压强度基本相同。变形后,Al2Y的形貌几乎没有变化,而LPSO发生了明显的扭结变形。温度的升高有利于DRX的发生。合金的DRX机制主要包括不连续动态再结晶(DDRX)和连续动态再结晶(CDRX),以DDRX为主。晶界处致密的板层状LPSO不利于DDRX的发生。变形后的显微组织呈现出典型的[0001]//CD(压缩方向)织构。随着温度的升高,由于多滑移体系的激活和DRX分数的增加,织构强度逐渐降低。在应变速率为0.01 s−1时,当温度升高到450℃时,变形晶粒数以金字塔形Ⅱ<c+a>滑差大幅增加。
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来源期刊
Journal of Alloys and Compounds
Journal of Alloys and Compounds 工程技术-材料科学:综合
CiteScore
11.10
自引率
14.50%
发文量
5146
审稿时长
67 days
期刊介绍: The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.
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