Residual stress characterization of dissimilar Ti/Al spot welds: A comparative study using synchrotron X-ray and neutron diffraction

IF 6.2 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING
Materials Characterization Pub Date : 2026-10-01 Epub Date: 2026-10-02 DOI:10.1016/j.matchar.2026.117153
Sanjay C. Krishnamurthy, Lasse Malaske, David Canelo-Yubero, Marc-André Nielsen, Thilo Pirling, Marie-Noëlle Avettand-Fènoël, Aude Simar, Benjamin Klusemann
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Abstract

Residual stress (RS) plays a critical role in the structural integrity of dissimilar titanium/aluminum (Ti/Al) spot welds, yet its reliable determination and interpretation remain challenging due to strong microstructural heterogeneity and steep stress gradients. In this study, RS distributions in Ti/Al spot welds produced by refill friction stir spot welding (refill FSSW) and spot friction melt bonding (FMB) are investigated using Neutron Diffraction (ND) and Energy-Dispersive Synchrotron X-Ray Diffraction (EDXRD). This work provides an original study on the quantification of RS using diffraction-based methods in dissimilar Ti/Al spot welds and presents a direct comparison between ND and EDXRD to assess their respective capabilities for RS determination. The results show that RS evolution is strongly dependent on the joining process. In spot FMB, RS is dominated by thermally induced stresses in the Ti, where constrained thermal contraction leads to high stress magnitudes and steep through-thickness gradients. In contrast, refill FSSW leads to a more uniform RS distribution owing to homogeneous deformation in the Al and limited influence of the process on the Ti. The comparison between ND and EDXRD reveals differences in the measured RS distributions, particularly in regions with steep gradients and pronounced microstructural heterogeneity, where spatial averaging effects influence ND measurements. In refill FSSW welds, where the microstructure is more homogeneous, both techniques show comparable RS trends. These findings provide new insights into the relationship between welding process, microstructure, and RS evolution in dissimilar Ti/Al joints.
不同Ti/Al点焊残余应力表征:同步x射线和中子衍射的对比研究
残余应力(RS)对异种钛/铝(Ti/Al)点焊的结构完整性起着至关重要的作用,但由于显微组织不均匀性强和应力梯度陡,残余应力的可靠测定和解释仍然具有挑战性。利用中子衍射(ND)和能量色散同步x射线衍射(EDXRD)研究了再填充搅拌摩擦点焊(fill - FSSW)和点摩擦熔体键合(FMB)制备的Ti/Al点焊中的RS分布。这项工作提供了在不同Ti/Al点焊中使用基于衍射的方法定量RS的原始研究,并提出了ND和EDXRD之间的直接比较,以评估它们各自的RS测定能力。结果表明,RS的演化强烈依赖于接合过程。在现场FMB中,RS主要由Ti中的热诱导应力主导,其中受约束的热收缩导致高应力值和陡峭的通过厚度梯度。相比之下,由于Al的变形均匀且工艺对Ti的影响有限,填充FSSW导致RS分布更加均匀。ND和EDXRD的比较揭示了测得的RS分布的差异,特别是在陡峭的梯度和明显的微观结构非均质性区域,空间平均效应影响ND测量。在填充FSSW焊缝中,微观结构更加均匀,两种技术都显示出相当的RS趋势。这些发现为不同Ti/Al接头的焊接工艺、显微组织和RS演化之间的关系提供了新的见解。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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