A Comparative Evaluation and a Benefit Assessment of Sintering α-Al2O3 in Induction and Conventional Furnaces

IF 2.6 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS
Hugo Barragán Vargas, María Camila Belduque Correa, Paulina López Eligio, Fernando Álvarez Ramirez, Ivanovich Estrada Guel, Ricardo Cuenca Álvarez, Francisco C. Robles Hernandez
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Abstract

This work provides a quantitative comparison of induction heating and conventional resistance-furnace sintering for the processing of high-purity α-Al2O3 ceramics, focusing on thermal behavior, energy efficiency, and sintering quality. The study combines experimental characterization of sintering samples and analysis of thermal curves. Here is also covered an energy-based modeling to propose a microstructural development, heating behavior, and overall energy demand for induction and conventional resistance furnaces. The materials used in this work are commercial alumina (as-received) and milled powder to isolate the effect of the heating method, with a mechanically milled condition. We also examined its influence on microstructure. The samples sintered by induction heating achieved a maximum relative density of ∼98.2% and a Vickers hardness of 2060 ± 22 HV at 1500°C for milled alumina powder, compared to 1980 ± 28 HV and 97.1% relative density for conventional sintering under identical conditions. Thermal simulations in a Matlab-based finite differences methods (FDM) model reveal that resistance-furnace heating is dominated by slow radiative and convective fluxes, leading to a slower achievement of a homogeneous temperature distribution, which in practice means the system takes longer to equilibrate. In induction heating, the sintering starts in the first few minutes and the pellet edges exhibit a more pronounced temperature rise. However, this condition diminishes rapidly, and within a short time the temperature distribution becomes homogeneous, achieving uniformity significantly faster than in a conventional furnace. Energy analysis shows that induction reduces total cumulative electrical consumption by 92.37% relative to the furnace at the highest target temperature evaluated (1500°C).

感应炉与常规炉烧结α-Al2O3的对比评价及效益评价
这项工作提供了感应加热和传统电阻炉烧结加工高纯度α-Al2O3陶瓷的定量比较,重点关注热行为,能源效率和烧结质量。本研究将烧结试样的实验表征与热曲线分析相结合。这里还涵盖了基于能量的建模,以提出微观结构的发展,加热行为,以及感应炉和传统电阻炉的总体能源需求。在这项工作中使用的材料是商业氧化铝(接收)和研磨粉末,以隔离加热方法的影响,机械研磨条件。我们还研究了其对微观结构的影响。在1500°C时,感应加热烧结的氧化铝粉末的最大相对密度为~ 98.2%,维氏硬度为2060±22 HV,而在相同条件下,常规烧结的相对密度为1980±28 HV,相对密度为97.1%。基于matlab的有限差分方法(FDM)模型的热模拟表明,电阻炉加热主要由缓慢的辐射和对流通量主导,导致温度分布均匀的速度较慢,这在实践中意味着系统需要更长的时间来平衡。在感应加热中,烧结在最初的几分钟内开始,颗粒边缘表现出更明显的温升。然而,这种情况迅速消失,在短时间内温度分布变得均匀,比在传统炉中更快地达到均匀性。能量分析表明,在评估的最高目标温度(1500°C)下,相对于炉体,感应减少了92.37%的累计总电耗。
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来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
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