Columnar to Equiaxed Transition in Electron Beam Powder Bed Fusion (EB-PBF) Characterized Through Microstructure Analytics

IF 3.6 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Advanced Engineering Materials Pub Date : 2026-09-11 Epub Date: 2026-03-27 DOI:10.1002/adem.202503160
Pascal Thome, Micheal Madigan, Shadman Tahsin Nabil, Owen Lowerey, Francisco Medina, Sammy Tin
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Abstract

Electron beam powder bed fusion (EB-PBF) offers the possibility to tailor local thermal histories via electromagnetic beam steering, yet the resulting columnar to equiaxed transition (CET) in Ni-based superalloys remains incompletely quantified. In this work, the CET in IN718 processed by spot-melting EB-PBF is systematically mapped using a microstructure analytics framework built on orientation-corrected pseudo-3D EBSD. Three processing degrees of freedom are explored: beam current, dwell time, and scanning strategy. A global coordinate system is enforced across three orthogonal cross sections, enabling consistent evaluation of grain morphology, crystallographic texture, and lack of fusion (LOF) porosity via percentile-based aspect ratio, grain size, misorientation, and pore-fraction descriptors. At fixed beam energy, comparison of structured (snake, single-direction) and nonstructured (single-direction-shifted, stochastic) patterns demonstrates that increasing spatial and temporal randomness disrupts thermal field coherence, suppresses epitaxial grain extension, and promotes fine equiaxed morphologies. Extending the analysis to a two-dimensional beam-current-dwell-time matrix under stochastic spot melting, experimentally determined process maps reveal a narrow processing window in which defect-lean, equiaxed, and nearly isotropic microstructures are obtained. This window is bounded on one side by insufficient energy input causing LOF defects, and on the other by excessive energy input driving strong morphological and crystallographic texture and abnormal grain growth. The results demonstrate that dwell time primarily governs crystallographic texture, whereas beam current and dwell time jointly control grain morphology and defect formation.

电子束粉末床熔合(EB-PBF)中柱状到等轴转变的微观结构分析
电子束粉末床熔合(EB-PBF)提供了通过电磁束控制来调整局部热历史的可能性,但镍基高温合金中柱状到等轴转变(CET)的结果仍未完全量化。在这项工作中,使用建立在定向校正伪3d EBSD上的微观结构分析框架,系统地绘制了点熔EB-PBF处理的IN718中的CET。研究了三种加工自由度:光束电流、停留时间和扫描策略。在三个正交截面上执行全局坐标系统,通过基于百分位数的纵横比、晶粒尺寸、取向偏差和孔隙分数描述符,实现对晶粒形态、晶体结构和LOF孔隙度的一致评估。在固定束流能量下,结构化(蛇形,单向)和非结构化(单向位移,随机)模式的比较表明,增加空间和时间随机性会破坏热场相干性,抑制外延晶粒延伸,并促进精细等轴形态。将分析扩展到随机点熔化下的二维光束电流-停留时间矩阵,实验确定的工艺图揭示了一个狭窄的加工窗口,在该窗口中可以获得缺陷少、等轴和几乎各向同性的微观结构。这个窗口的一边是能量输入不足导致LOF缺陷,另一边是能量输入过多导致强烈的形态和晶体织构以及异常的晶粒生长。结果表明,停留时间主要控制晶体织构,而光束电流和停留时间共同控制晶粒形貌和缺陷形成。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Advanced Engineering Materials
Advanced Engineering Materials 工程技术-材料科学:综合
CiteScore
5.70
自引率
5.60%
发文量
544
审稿时长
1.7 months
期刊介绍: Advanced Engineering Materials is the membership journal of three leading European Materials Societies - German Materials Society/DGM, - French Materials Society/SF2M, - Swiss Materials Federation/SVMT.
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