Microstructure and Mechanical Response of Additively Manufactured Maraging Steel Modified by Heat Treatment

IF 4.5 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Van Loi Tran, Jeong-Rim Lee, Sang-Hun Lee, Dong-Hyun Kim, Sua Hong, Youngkyun Son, Jihwan Choi, Dong-Hyun Kim
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Abstract

This study investigated the effects of processing parameters and heat treatment on the densification, mechanical properties, and microstructure of maraging steel 1.2709 fabricated by laser powder bed fusion (PBF). A 5 × 5 matrix of process conditions was examined with laser power ranging from 180 to 220 W and scan speed from 700 to 1100 mm/s. The optimal condition was identified at 200 W and 700 mm/s, corresponding to an energy density of 79.4 J/mm3, which yielded a near-full density of 99.91% and superior tensile properties (UTS 1218.5 MPa, elongation 17.6%). Process parameter optimization improved densification by reducing porosity, thereby enhancing tensile strength and ductility. Notably, the fully martensitic structure of the as-built sample largely reverts to austenite, with only a trace amount (~ 30%) of BCC phase remaining, at a heat treatment temperature of 650 °C, leading to a significant strain-induced phase transformation of austenite (TRIP effect). Furthermore, furnace cooling produces relatively more stable reverted austenite, which suppresses immediate transformation at the onset of strain and thereby delays the TRIP effect, enabling extended work hardening and improved ductility of up to 24.3% while maintaining tensile strength above 1150 MPa compared to air cooling. These findings highlight a combined strategy of optimizing PBF parameters and tailoring intercritical heat treatment to control the TRIP effect, offering practical guidelines for the fabrication and commercialization of maraging steel 1.2709 with improved processability and mechanical performance.

Graphical abstract

Abstract Image

热处理改性马氏体时效钢的组织与力学响应
研究了工艺参数和热处理对激光粉末床熔合法制备马氏体时效钢1.2709的致密化、力学性能和显微组织的影响。在激光功率为180 ~ 220 W,扫描速度为700 ~ 1100 mm/s的条件下,研究了5 × 5的工艺条件矩阵。在200 W和700 mm/s下,能量密度为79.4 J/mm3,获得了99.91%的近满密度和优异的拉伸性能(UTS 1218.5 MPa,伸长率17.6%)。工艺参数优化通过降低孔隙率改善致密化,从而提高拉伸强度和延展性。值得注意的是,在650℃的热处理温度下,构建样品的完全马氏体结构大部分还原为奥氏体,仅残留微量(~ 30%)的BCC相,导致了明显的应变诱导奥氏体相变(TRIP效应)。此外,炉内冷却产生相对更稳定的还原奥氏体,这抑制了应变开始时的立即转变,从而延缓了TRIP效应,使加工硬化时间延长,延展性提高24.3%,同时与空气冷却相比,抗拉强度保持在1150 MPa以上。这些发现强调了优化PBF参数和定制临界间热处理以控制TRIP效应的组合策略,为改善加工性能和机械性能的马氏体时效钢1.2709的制造和商业化提供了实用指南。图形抽象
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来源期刊
Metals and Materials International
Metals and Materials International 工程技术-材料科学:综合
CiteScore
7.10
自引率
8.60%
发文量
197
审稿时长
3.7 months
期刊介绍: Metals and Materials International publishes original papers and occasional critical reviews on all aspects of research and technology in materials engineering: physical metallurgy, materials science, and processing of metals and other materials. Emphasis is placed on those aspects of the science of materials that are concerned with the relationships among the processing, structure and properties (mechanical, chemical, electrical, electrochemical, magnetic and optical) of materials. Aspects of processing include the melting, casting, and fabrication with the thermodynamics, kinetics and modeling.
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