Yan Victor Silva de Santana, Emanuel Ewerton Mendonça Vasconcelos, Gabriela Queiroz de Melo Monteiro, Agna Roberta Xavier Bezerra, Luís Felipe Espíndola-Castro
{"title":"Evaluation of physicomechanical and optical properties of bioactive glass (BAG)-filled resin composites: an <i>in vitro</i> study.","authors":"Yan Victor Silva de Santana, Emanuel Ewerton Mendonça Vasconcelos, Gabriela Queiroz de Melo Monteiro, Agna Roberta Xavier Bezerra, Luís Felipe Espíndola-Castro","doi":"10.2340/biid.v13.46233","DOIUrl":null,"url":null,"abstract":"<p><strong>Objective: </strong>To evaluate the behavior of bioactive glass (BAG)-filled resin composites (Beautifil II / Shofu-BR and Beautifil Flow Plus / Shofu-BF) compared with conventional resin composites (Filtek Z350 XT / Solventum-ZR and Filtek Supreme Flowable Restorative / Solventum-FS) by means of microhardness, sorption, solubility, and color stability tests.</p><p><strong>Materials and methods: </strong>For these analyses, ten specimens were fabricated per group using a split metal mold (15 mm in diameter × 1 mm thickness). Microhardness (<i>n</i> = 10) was measured using a digital microhardness tester, based on the mean of three indentations per specimen under a 2.94 N load for 15 s. For the sorption and solubility tests, five out of the 10 specimens used in the microhardness assays were randomly selected (<i>n</i> = 5), and ISO 4049/2019 recommendations were followed. Color stability was assessed using a digital spectrophotometer by comparing specimens immersed in coffee (using the five specimens not selected for the sorption and solubility tests / <i>n</i> = 5) and distilled water (control, using the same specimens from the sorption and solubility tests), with measurements obtained at baseline, after 1 day, and after 1 week of immersion. Color change (ΔE) was calculated using CIELAB parameters.</p><p><strong>Results: </strong>For microhardness, the high-viscosity resin composites (ZR and BR) showed significantly higher mean values than their low-viscosity versions (<i>p</i> < 0.001). Although sorption differed significantly among groups (<i>p</i> = 0.001), all resin composites exhibited values within the limits established by ISO 4049/2019. No statistically significant differences were observed for solubility. Regarding color stability, after 7 days in coffee, BR and ZR exhibited the greatest color changes (ΔE). Despite the observed statistical differences, the changes remained within acceptable clinical limits.</p><p><strong>Conclusion: </strong>BAG-filled resin composites exhibit properties comparable to those of conventional resin composites. The ZR resin composite showed higher microhardness; however, for the other evaluated parameters (sorption, solubility, and color stability in coffee), the tested resin composites exhibited values within the limits recommended by ISO 4049:2019 and were comparable to those of the reference conventional high- or low-viscosity resin composite.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":"65 ","pages":"46233"},"PeriodicalIF":0.0000,"publicationDate":"2026-06-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC13273812/pdf/","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Biomaterial investigations in dentistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2340/biid.v13.46233","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2026/1/1 0:00:00","PubModel":"eCollection","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Objective: To evaluate the behavior of bioactive glass (BAG)-filled resin composites (Beautifil II / Shofu-BR and Beautifil Flow Plus / Shofu-BF) compared with conventional resin composites (Filtek Z350 XT / Solventum-ZR and Filtek Supreme Flowable Restorative / Solventum-FS) by means of microhardness, sorption, solubility, and color stability tests.
Materials and methods: For these analyses, ten specimens were fabricated per group using a split metal mold (15 mm in diameter × 1 mm thickness). Microhardness (n = 10) was measured using a digital microhardness tester, based on the mean of three indentations per specimen under a 2.94 N load for 15 s. For the sorption and solubility tests, five out of the 10 specimens used in the microhardness assays were randomly selected (n = 5), and ISO 4049/2019 recommendations were followed. Color stability was assessed using a digital spectrophotometer by comparing specimens immersed in coffee (using the five specimens not selected for the sorption and solubility tests / n = 5) and distilled water (control, using the same specimens from the sorption and solubility tests), with measurements obtained at baseline, after 1 day, and after 1 week of immersion. Color change (ΔE) was calculated using CIELAB parameters.
Results: For microhardness, the high-viscosity resin composites (ZR and BR) showed significantly higher mean values than their low-viscosity versions (p < 0.001). Although sorption differed significantly among groups (p = 0.001), all resin composites exhibited values within the limits established by ISO 4049/2019. No statistically significant differences were observed for solubility. Regarding color stability, after 7 days in coffee, BR and ZR exhibited the greatest color changes (ΔE). Despite the observed statistical differences, the changes remained within acceptable clinical limits.
Conclusion: BAG-filled resin composites exhibit properties comparable to those of conventional resin composites. The ZR resin composite showed higher microhardness; however, for the other evaluated parameters (sorption, solubility, and color stability in coffee), the tested resin composites exhibited values within the limits recommended by ISO 4049:2019 and were comparable to those of the reference conventional high- or low-viscosity resin composite.