Effect of light attenuation on curing performance of ZrO2 ceramic for stereolithography

IF 2.5 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
Y. B. Liu, Jinqiang Zhou, Jianwei Zhang, Jianguo Cheng, Lina Zhan
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引用次数: 0

Abstract

Abstract The attenuation coefficient of ultraviolet UV light is a critical factor influencing the mechanical properties of photocurable ceramics. Aiming to fabricate high-precision and high-performance ZrO 2 ceramics, this study systematically investigates the impact of the UV attenuation coefficient on the polymerization kinetics of ZrO 2 ceramic slurries. Through linear fitting, the absorption and scattering coefficients of the ZrO 2 slurry were determined as 66 cm −1 . By integrating the Beer-Lambert law, we further validated how the UV attenuation coefficient affects the variation in C=C double bond conversion within the cured slurry layers. Additionally, based on Mie scattering theory, although the incident energy was 52 mW cm −2 and slice thickness was 50 μm, the curing depth C d and exposure energy I n E o is optimal. The ZrO 2 ceramic was formed , in which the sintered sample density was 6.02 g cm −3 (99%).
光衰减对ZrO2陶瓷固化性能的影响
摘要紫外光的衰减系数是影响光固化陶瓷力学性能的关键因素。以制备高精度高性能的ZrO - 2陶瓷为目标,系统研究了紫外光衰减系数对ZrO - 2陶瓷浆料聚合动力学的影响。通过线性拟合,确定了zro2浆料的吸收和散射系数为66 cm−1。通过对Beer-Lambert定律的积分,我们进一步验证了UV衰减系数如何影响固化浆料层内C=C双键转换的变化。此外,基于Mie散射理论,当入射能量为52 mW cm−2,薄片厚度为50 μm时,固化深度C d和暴露能量I n E o是最优的。制备了zro2陶瓷,烧结样品密度为6.02 g cm−3(99%)。
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来源期刊
Materials Research Express
Materials Research Express MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
4.50
自引率
4.30%
发文量
640
审稿时长
12 weeks
期刊介绍: A broad, rapid peer-review journal publishing new experimental and theoretical research on the design, fabrication, properties and applications of all classes of materials.
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